(E)-(SR)-N-methyl-N-<6-(2,4,6-triisopropylphenylsulfinyl)hex-5-en-1-yl>trifluoroacetamide

Base Information

Chemical Name:(E)-(SR)-N-methyl-N-<6-(2,4,6-triisopropylphenylsulfinyl)hex-5-en-1-yl>trifluoroacetamide
CAS No.:123934-70-3
Molecular Formula:C₂₄H₃₆F₃NO₂S
Molecular Weight:459.617
Hs Code.:

Synonyms:(E)-(SR)-N-methyl-N-<6-(2,4,6-triisopropylphenylsulfinyl)hex-5-en-1-yl>trifluoroacetamide

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Chemical Property of (E)-(SR)-N-methyl-N-<6-(2,4,6-triisopropylphenylsulfinyl)hex-5-en-1-yl>trifluoroacetamide

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Technology Process of (E)-(SR)-N-methyl-N-<6-(2,4,6-triisopropylphenylsulfinyl)hex-5-en-1-yl>trifluoroacetamide

There total 5 articles about (E)-(SR)-N-methyl-N-<6-(2,4,6-triisopropylphenylsulfinyl)hex-5-en-1-yl>trifluoroacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2508-29-4
5-hydroxypentylamine

: 123934-70-3
(E)-(SR)-N-methyl-N-<6-(2,4,6-triisopropylphenylsulfinyl)hex-5-en-1-yl>trifluoroacetamide

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / CH₂Cl₂; pyridine / 0 dec C, 10 min, then room temp., 45 min

2: 63 percent / KOH / acetone / 0.08 h / Heating

3: 92 percent / PCC / CH₂Cl₂ / 2 h / Ambient temperature

4: 1.) nBuLi / 1.) THF, -78 deg C, 2h, 2.) -78 deg C, 2h, then room temp., 2h

With potassium hydroxide; n-butyllithium; pyridinium chlorochromate; In pyridine; dichloromethane; acetone;
DOI:10.1021/jo00290a051

Reference yield:

: 123934-63-4
N-methyl-N-(5-hydroxy-1-pentyl)trifluoroacetamide

: 123934-70-3
(E)-(SR)-N-methyl-N-<6-(2,4,6-triisopropylphenylsulfinyl)hex-5-en-1-yl>trifluoroacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / PCC / CH₂Cl₂ / 2 h / Ambient temperature

2: 1.) nBuLi / 1.) THF, -78 deg C, 2h, 2.) -78 deg C, 2h, then room temp., 2h

With n-butyllithium; pyridinium chlorochromate; In dichloromethane;
DOI:10.1021/jo00290a051

Reference yield:

: 123934-62-3
5-(trifluoroacetamido)pentyl trifluoroacetate

: 123934-70-3
(E)-(SR)-N-methyl-N-<6-(2,4,6-triisopropylphenylsulfinyl)hex-5-en-1-yl>trifluoroacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 63 percent / KOH / acetone / 0.08 h / Heating

2: 92 percent / PCC / CH₂Cl₂ / 2 h / Ambient temperature

3: 1.) nBuLi / 1.) THF, -78 deg C, 2h, 2.) -78 deg C, 2h, then room temp., 2h

With potassium hydroxide; n-butyllithium; pyridinium chlorochromate; In dichloromethane; acetone;
DOI:10.1021/jo00290a051