2-((2,4-dichlorobenzyl)oxy)benzaldehyde O-(1-methylpyrrolidin-3-yl) oxime

Base Information

Chemical Name:2-((2,4-dichlorobenzyl)oxy)benzaldehyde O-(1-methylpyrrolidin-3-yl) oxime
CAS No.:1430842-09-3
Molecular Formula:C₁₉H₂₀Cl₂N₂O₂
Molecular Weight:379.286
Hs Code.:

Synonyms:2-((2,4-dichlorobenzyl)oxy)benzaldehyde O-(1-methylpyrrolidin-3-yl) oxime

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Chemical Property of 2-((2,4-dichlorobenzyl)oxy)benzaldehyde O-(1-methylpyrrolidin-3-yl) oxime

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Technology Process of 2-((2,4-dichlorobenzyl)oxy)benzaldehyde O-(1-methylpyrrolidin-3-yl) oxime

There total 4 articles about 2-((2,4-dichlorobenzyl)oxy)benzaldehyde O-(1-methylpyrrolidin-3-yl) oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

: 52803-60-8
2-(2,4-dichlorobenzyloxy)benzaldehyde

: O-(1-methylpyrrolidin-3-yl)hydroxylamine hydrogen chloride

: 1430842-09-3
2-((2,4-dichlorobenzyl)oxy)benzaldehyde O-(1-methylpyrrolidin-3-yl) oxime

Guidance literature:: With sodium carbonate; In methanol; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1016/j.ejmech.2012.12.033

Reference yield:

: 793642-23-6
O-(1-methylpyrrolidin-3-yl)hydroxylamine

: 1430842-09-3
2-((2,4-dichlorobenzyl)oxy)benzaldehyde O-(1-methylpyrrolidin-3-yl) oxime

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / water / Inert atmosphere

2: sodium carbonate / methanol / 3 h / 20 °C / Inert atmosphere

With hydrogenchloride; sodium carbonate; In methanol; water;
DOI:10.1016/j.ejmech.2012.12.033

Reference yield:

: 13220-33-2,99445-21-3
1-methyl-3-pyrrolidinol

: 1430842-09-3
2-((2,4-dichlorobenzyl)oxy)benzaldehyde O-(1-methylpyrrolidin-3-yl) oxime

Guidance literature:: Multi-step reaction with 4 steps

1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 6 h / 0 °C / Inert atmosphere

2: hydrazine hydrate / ethanol / 3 h / 80 °C / Inert atmosphere

3: hydrogenchloride / water / Inert atmosphere

4: sodium carbonate / methanol / 3 h / 20 °C / Inert atmosphere

With hydrogenchloride; di-isopropyl azodicarboxylate; sodium carbonate; hydrazine hydrate; triphenylphosphine; In tetrahydrofuran; methanol; ethanol; water;
DOI:10.1016/j.ejmech.2012.12.033