(1H)-2-thioxo-1-pyridyl 3-(diphenylphosphatoxy)-2-methoxy-2-methyl-3-phenylpropionate

Base Information

Chemical Name:(1H)-2-thioxo-1-pyridyl 3-(diphenylphosphatoxy)-2-methoxy-2-methyl-3-phenylpropionate
CAS No.:343986-67-4
Molecular Formula:C₂₈H₂₆NO₇PS
Molecular Weight:551.557
Hs Code.:

Synonyms:(1H)-2-thioxo-1-pyridyl 3-(diphenylphosphatoxy)-2-methoxy-2-methyl-3-phenylpropionate

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Chemical Property of (1H)-2-thioxo-1-pyridyl 3-(diphenylphosphatoxy)-2-methoxy-2-methyl-3-phenylpropionate

Chemical Property:

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Technology Process of (1H)-2-thioxo-1-pyridyl 3-(diphenylphosphatoxy)-2-methoxy-2-methyl-3-phenylpropionate

There total 3 articles about (1H)-2-thioxo-1-pyridyl 3-(diphenylphosphatoxy)-2-methoxy-2-methyl-3-phenylpropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3696-28-4
2,2'-dipyridyl disulfide bis-N-oxide

: 343986-66-3
3-(diphenylphosphatoxy)-2-methoxy-2-methyl-3-phenylpropionic acid

: 343986-67-4
(1H)-2-thioxo-1-pyridyl 3-(diphenylphosphatoxy)-2-methoxy-2-methyl-3-phenylpropionate

Guidance literature:: With triphenylphosphine; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1021/ja0042938

Reference yield:

: 343986-64-1
2,4-dimethoxybenzyl 3-hydroxy-2-methoxy-2-methyl-3-phenylpropionate

: 343986-67-4
(1H)-2-thioxo-1-pyridyl 3-(diphenylphosphatoxy)-2-methoxy-2-methyl-3-phenylpropionate

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / DMAP / CH₂Cl₂ / 14 h / 20 °C

2: ceric ammonium nitrate / H₂O; acetonitrile / 1 h / 20 °C

3: 0.204 g / PPh₃ / CH₂Cl₂ / 1 h / 20 °C

With dmap; ammonium cerium(IV) nitrate; triphenylphosphine; In dichloromethane; water; acetonitrile; 3: Mitsunobu reaction;
DOI:10.1021/ja0042938

Reference yield:

: 343986-65-2
2,4-dimethoxybenzyl 3-(diphenyl-phosphatoxy)-2-methoxy-2-methyl-3-phenylpropionate

: 343986-67-4
(1H)-2-thioxo-1-pyridyl 3-(diphenylphosphatoxy)-2-methoxy-2-methyl-3-phenylpropionate

Guidance literature:: Multi-step reaction with 2 steps

1: ceric ammonium nitrate / H₂O; acetonitrile / 1 h / 20 °C

2: 0.204 g / PPh₃ / CH₂Cl₂ / 1 h / 20 °C

With ammonium cerium(IV) nitrate; triphenylphosphine; In dichloromethane; water; acetonitrile; 2: Mitsunobu reaction;
DOI:10.1021/ja0042938