2,4-dimethoxybenzyl 3-(diphenyl-phosphatoxy)-2-methoxy-2-methyl-3-phenylpropionate

Base Information

Chemical Name:2,4-dimethoxybenzyl 3-(diphenyl-phosphatoxy)-2-methoxy-2-methyl-3-phenylpropionate
CAS No.:343986-65-2
Molecular Formula:C₃₂H₃₃O₉P
Molecular Weight:592.582
Hs Code.:

Synonyms:2,4-dimethoxybenzyl 3-(diphenyl-phosphatoxy)-2-methoxy-2-methyl-3-phenylpropionate

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Chemical Property of 2,4-dimethoxybenzyl 3-(diphenyl-phosphatoxy)-2-methoxy-2-methyl-3-phenylpropionate

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Technology Process of 2,4-dimethoxybenzyl 3-(diphenyl-phosphatoxy)-2-methoxy-2-methyl-3-phenylpropionate

There total 2 articles about 2,4-dimethoxybenzyl 3-(diphenyl-phosphatoxy)-2-methoxy-2-methyl-3-phenylpropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 2524-64-3
chlorophosphoric acid diphenyl ester

: 343986-64-1
2,4-dimethoxybenzyl 3-hydroxy-2-methoxy-2-methyl-3-phenylpropionate

: 343986-65-2
2,4-dimethoxybenzyl 3-(diphenyl-phosphatoxy)-2-methoxy-2-methyl-3-phenylpropionate

Guidance literature:: With dmap; In dichloromethane; at 20 ℃; for 14h;
DOI:10.1021/ja0042938

Reference yield:

: 343986-63-0
2,4-dimethoxybenzyl 2-methoxypropionate

: 343986-65-2
2,4-dimethoxybenzyl 3-(diphenyl-phosphatoxy)-2-methoxy-2-methyl-3-phenylpropionate

Guidance literature:: Multi-step reaction with 2 steps

1.1: diisopropylamine; n-BuLi / tetrahydrofuran; cyclohexane / 0.5 h / -78 °C

1.2: 92 percent / tetrahydrofuran; cyclohexane / 1.5 h / -78 °C

2.1: 81 percent / DMAP / CH₂Cl₂ / 14 h / 20 °C

With dmap; n-butyllithium; diisopropylamine; In tetrahydrofuran; dichloromethane; cyclohexane;
DOI:10.1021/ja0042938