4-(Dichloromethyl)benzoyl chloride

Base Information

Chemical Name:4-(Dichloromethyl)benzoyl chloride
CAS No.:36747-64-5
Molecular Formula:C8H5 Cl3 O
Molecular Weight:223.486
Hs Code.:2916399090
European Community (EC) Number:622-777-0
DSSTox Substance ID:DTXSID10455446
Wikidata:Q82277435
Mol file:36747-64-5.mol

Synonyms:4-(Dichloromethyl)benzoyl chloride;36747-64-5;SCHEMBL9681747;DTXSID10455446;AKOS015889271

Suppliers and Price of 4-(Dichloromethyl)benzoyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 21 raw suppliers

Chemical Property of 4-(Dichloromethyl)benzoyl chloride

Chemical Property:

Melting Point:50-55 °C(lit.)
Boiling Point:285-286 °C(Press: 745 Torr)
Flash Point:>230 °F
PSA：17.07000
Density:1.435±0.06 g/cm3(Predicted)
LogP:3.54180
XLogP3:3.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:221.940598
Heavy Atom Count:12
Complexity:162

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:C
Statements: 34
Safety Statements: 26-36/37/39-45

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1C(Cl)Cl)C(=O)Cl

Technology Process of 4-(Dichloromethyl)benzoyl chloride

There total 8 articles about 4-(Dichloromethyl)benzoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 874-60-2
4-methyl-benzoyl chloride

: 36747-64-5
4-(dichloromethyl)benzoyl chloride

Guidance literature:: With Perbenzoic acid; chlorine; In tetrachloromethane; for 6h; Heating;
DOI:10.1002/jps.2600710115

Reference yield:

: 619-66-9
4-Carboxybenzaldehyde

: 36747-64-5
4-(dichloromethyl)benzoyl chloride

Guidance literature:: With phosphorus pentachloride;

Reference yield:

: 99-94-5
p-Toluic acid

: 36747-64-5
4-(dichloromethyl)benzoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride

2: 86 percent / Cl₂, benzoyl peroxide / CCl₄ / 6 h / Heating

With thionyl chloride; Perbenzoic acid; chlorine; In tetrachloromethane;
DOI:10.1002/jps.2600710115