C₃₀H₅₆O₃Si

Base Information

Chemical Name:C₃₀H₅₆O₃Si
CAS No.:942137-27-1
Molecular Formula:C₃₀H₅₆O₃Si
Molecular Weight:492.858
Hs Code.:

C<sub>30</sub>H<sub>56</sub>O<sub>3</sub>Si

Synonyms:C₃₀H₅₆O₃Si

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Chemical Property of C₃₀H₅₆O₃Si

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Technology Process of C₃₀H₅₆O₃Si

There total 1 articles about C₃₀H₅₆O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 942137-26-0
C₂₄H₄₂O₃

: 18162-48-6
tert-butyldimethylsilyl chloride

: 942137-27-1
C₃₀H₅₆O₃Si

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1016/j.tetlet.2007.03.115

Reference yield:

: 942137-27-1
C₃₀H₅₆O₃Si

: 942137-30-6
C₃₅H₆₅NO₄Si

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 0 - 20 °C

2: 86 percent / NaN₃ / dimethylformamide / Heating

3: 87 percent / Ph₃P / methanol / Heating

4: 93 percent / triethylamine; 4,4-dimethylaminopyridine / tetrahydrofuran / 20 °C

With pyridine; dmap; sodium azide; triethylamine; triphenylphosphine; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2007.03.115

Reference yield:

: 942137-27-1
C₃₀H₅₆O₃Si

: C₂₉H₅₁NO₄

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / 0 - 20 °C

2: 86 percent / NaN₃ / dimethylformamide / Heating

3: 87 percent / Ph₃P / methanol / Heating

4: 93 percent / triethylamine; 4,4-dimethylaminopyridine / tetrahydrofuran / 20 °C

5: 97 percent / tetrabutylammonium fluoride / tetrahydrofuran / -78 °C

With pyridine; dmap; sodium azide; tetrabutyl ammonium fluoride; triethylamine; triphenylphosphine; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2007.03.115