C₁₅H₁₅NO₄S₂

Base Information

Chemical Name:C₁₅H₁₅NO₄S₂
CAS No.:1433218-58-6
Molecular Formula:C₁₅H₁₅NO₄S₂
Molecular Weight:337.42
Hs Code.:

C<sub>15</sub>H<sub>15</sub>NO<sub>4</sub>S<sub>2</sub>

Synonyms:C₁₅H₁₅NO₄S₂

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Chemical Property of C₁₅H₁₅NO₄S₂

Chemical Property:

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Technology Process of C₁₅H₁₅NO₄S₂

There total 10 articles about C₁₅H₁₅NO₄S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 338777-79-0
4-tosyl-3,4-dihydro-2H-benzo[b][1,4]thiazine

: 1433218-58-6
C₁₅H₁₅NO₄S₂

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; for 3h;
DOI:10.1021/ol400618k

Reference yield:

: 1433218-59-7
N-(2-iodoethyl)-N-(2-iodophenyl)-4-methylbenzenesulfonamide

: 1433218-58-6
C₁₅H₁₅NO₄S₂

Guidance literature:: Multi-step reaction with 2 steps

1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; 1,1'-bis-(diphenylphosphino)ferrocene; caesium carbonate; Sodium thiosulfate pentahydrate; tetrabutylammomium bromide / acetonitrile; water / 6 h / 150 °C / Sealed tube; Inert atmosphere

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / 0 °C

With 1,1'-bis-(diphenylphosphino)ferrocene; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; Sodium thiosulfate pentahydrate; tetrabutylammomium bromide; caesium carbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; water; acetonitrile;
DOI:10.1021/ol400618k

Reference yield:

: 615-43-0
2-iodophenylamine

: 1433218-58-6
C₁₅H₁₅NO₄S₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridine / 5 h / 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h

2.2: 8 h / 80 °C

3.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; 1,1'-bis-(diphenylphosphino)ferrocene; caesium carbonate; Sodium thiosulfate pentahydrate; tetrabutylammomium bromide / acetonitrile; water / 8 h / 150 °C / Sealed tube; Inert atmosphere

4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / 0 °C

With 1,1'-bis-(diphenylphosphino)ferrocene; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; Sodium thiosulfate pentahydrate; tetrabutylammomium bromide; sodium hydride; caesium carbonate; 3-chloro-benzenecarboperoxoic acid; In pyridine; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ol400618k