C₃₂H₂₄ClNO₃

Base Information

Chemical Name:C₃₂H₂₄ClNO₃
CAS No.:1582776-46-2
Molecular Formula:C₃₂H₂₄ClNO₃
Molecular Weight:506
Hs Code.:

C<sub>32</sub>H<sub>24</sub>ClNO<sub>3</sub>

Synonyms:C₃₂H₂₄ClNO₃

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Chemical Property of C₃₂H₂₄ClNO₃

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Technology Process of C₃₂H₂₄ClNO₃

There total 5 articles about C₃₂H₂₄ClNO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 874831-02-4
ethyl 3-chloro-4-iodobenzoate

: 1582776-34-8
5,8-diphenyl-2-naphthamide

: 1582776-46-2
C₃₂H₂₄ClNO₃

Guidance literature:: With copper(l) iodide; (S,S)-1,2-diaminocyclohexane; potassium carbonate; In 1,4-dioxane; at 140 ℃; for 17h; Sealed tube;
DOI:10.1021/ml400521f

Reference yield:

: 2459-25-8
methyl naphthalene-2-carboxylate

: 1582776-46-2
C₃₂H₂₄ClNO₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: trifluorormethanesulfonic acid; bis-(pyridine)iodonium(I) tetrafluoroborate / dichloromethane / 22 h / 25 °C

2.1: triphenylphosphine; sodium carbonate / tetrahydrofuran; water / 110 °C / Microwave irradiation

3.1: potassium hydroxide / methanol; water / 3 h / 50 °C

4.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 3 h / 25 °C

4.2: 2.5 h / 0 - 25 °C

5.1: (S,S)-1,2-diaminocyclohexane; potassium carbonate; copper(l) iodide / 1,4-dioxane / 17 h / 140 °C / Sealed tube

With copper(l) iodide; trifluorormethanesulfonic acid; bis-(pyridine)iodonium(I) tetrafluoroborate; (S,S)-1,2-diaminocyclohexane; sodium carbonate; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triphenylphosphine; potassium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ml400521f

Reference yield:

: 1582776-31-5
methyl 5,8-diphenyl-2-naphthoate

: 1582776-46-2
C₃₂H₂₄ClNO₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium hydroxide / methanol; water / 3 h / 50 °C

2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 3 h / 25 °C

2.2: 2.5 h / 0 - 25 °C

3.1: (S,S)-1,2-diaminocyclohexane; potassium carbonate; copper(l) iodide / 1,4-dioxane / 17 h / 140 °C / Sealed tube

With copper(l) iodide; (S,S)-1,2-diaminocyclohexane; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; potassium hydroxide; In 1,4-dioxane; methanol; water; N,N-dimethyl-formamide;
DOI:10.1021/ml400521f