N-methyl-N-(4-methyl-5-phenyl-4,5-dihydrobenzo[d]oxepin-2-yl)methanesulfonamide

Base Information

Chemical Name:N-methyl-N-(4-methyl-5-phenyl-4,5-dihydrobenzo[d]oxepin-2-yl)methanesulfonamide
CAS No.:1402850-47-8
Molecular Formula:C₁₉H₂₁NO₃S
Molecular Weight:343.447
Hs Code.:

Synonyms:N-methyl-N-(4-methyl-5-phenyl-4,5-dihydrobenzo[d]oxepin-2-yl)methanesulfonamide

Suppliers and Price of N-methyl-N-(4-methyl-5-phenyl-4,5-dihydrobenzo[d]oxepin-2-yl)methanesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-methyl-N-(4-methyl-5-phenyl-4,5-dihydrobenzo[d]oxepin-2-yl)methanesulfonamide

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Technology Process of N-methyl-N-(4-methyl-5-phenyl-4,5-dihydrobenzo[d]oxepin-2-yl)methanesulfonamide

There total 1 articles about N-methyl-N-(4-methyl-5-phenyl-4,5-dihydrobenzo[d]oxepin-2-yl)methanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1333483-14-9
N-methyll-N-(phenylethylnyl)methanesulfonamide

: 14212-53-4
(1S,2R)-cis-methylstyrene oxide

: 1402850-47-8
N-methyl-N-(4-methyl-5-phenyl-4,5-dihydrobenzo[d]oxepin-2-yl)methanesulfonamide

Guidance literature:: With chloro(1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene)gold(I); silver(I) triflimide; In dichloromethane; at 28 ℃; optical yield given as %ee; chemoselective reaction; Inert atmosphere;
DOI:10.1002/anie.201203723

Reference yield: 85.0%

: 1402850-47-8
N-methyl-N-(4-methyl-5-phenyl-4,5-dihydrobenzo[d]oxepin-2-yl)methanesulfonamide

: 1402850-48-9
4-methyl-5-phenyl-4,5-dihydrobenzo[d]oxepin-2(1H)-one

Guidance literature:: With trifluorormethanesulfonic acid; In dichloromethane; at 0 ℃; for 5h; optical yield given as %ee; Inert atmosphere;
DOI:10.1002/anie.201203723