C₃₅H₃₈Cl₃NO₁₀

Base Information

Chemical Name:C₃₅H₃₈Cl₃NO₁₀
CAS No.:1577228-16-0
Molecular Formula:C₃₅H₃₈Cl₃NO₁₀
Molecular Weight:739.046
Hs Code.:

C<sub>35</sub>H<sub>38</sub>Cl<sub>3</sub>NO<sub>10</sub>

Synonyms:C₃₅H₃₈Cl₃NO₁₀

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Chemical Property of C₃₅H₃₈Cl₃NO₁₀

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Technology Process of C₃₅H₃₈Cl₃NO₁₀

There total 7 articles about C₃₅H₃₈Cl₃NO₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₃H₃₈O₁₀

: 545-06-2
trichloroacetonitrile

: 1577228-16-0
C₃₅H₃₈Cl₃NO₁₀

Guidance literature:: With sodium hydride; In dichloromethane; at 20 ℃; for 1.5h; Inert atmosphere;
DOI:10.1039/c3ob42312c

Reference yield:

: 1577227-58-7
dimethylthexylsilyl 3-O-benzyl-4,6-di-O-benzylidene-β-D-glucopyranoside

: 1577228-16-0
C₃₅H₃₈Cl₃NO₁₀

Guidance literature:: Multi-step reaction with 6 steps

1.1: pyridine; dmap / 4 h / 0 - 20 °C / Inert atmosphere

2.1: ethanethiol; toluene-4-sulfonic acid / dichloromethane; water / 1 h / 20 °C / Inert atmosphere

3.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane; water / 20 °C / Inert atmosphere

3.2: Inert atmosphere

4.1: sodium hydride; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 0.5 h / -20 °C / Inert atmosphere

5.1: pyridine hydrogenfluoride / tetrahydrofuran / 18 h / Inert atmosphere

6.1: sodium hydride / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

With pyridine; dmap; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; tetra-(n-butyl)ammonium iodide; sodium hydride; toluene-4-sulfonic acid; pyridine hydrogenfluoride; ethanethiol; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1039/c3ob42312c

Reference yield:

: 1577227-74-7
dimethylthexylsilyl O-methyl-2-O-(4-acetoxy-2,2-dimethylbutanoate)-3-O-benzyl-β-D-glucopyranosyluronate

: 1577228-16-0
C₃₅H₃₈Cl₃NO₁₀

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 0.5 h / -20 °C / Inert atmosphere

2: pyridine hydrogenfluoride / tetrahydrofuran / 18 h / Inert atmosphere

3: sodium hydride / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

With tetra-(n-butyl)ammonium iodide; sodium hydride; pyridine hydrogenfluoride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c3ob42312c