(E)-methyl 2-(2-bromo-3-methoxy-5-methylbenzylidene)-6-methylhept-5-enoate

Base Information

Chemical Name:(E)-methyl 2-(2-bromo-3-methoxy-5-methylbenzylidene)-6-methylhept-5-enoate
CAS No.:1134789-26-6
Molecular Formula:C₁₈H₂₃BrO₃
Molecular Weight:367.283
Hs Code.:

Synonyms:(E)-methyl 2-(2-bromo-3-methoxy-5-methylbenzylidene)-6-methylhept-5-enoate

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Chemical Property of (E)-methyl 2-(2-bromo-3-methoxy-5-methylbenzylidene)-6-methylhept-5-enoate

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Technology Process of (E)-methyl 2-(2-bromo-3-methoxy-5-methylbenzylidene)-6-methylhept-5-enoate

There total 1 articles about (E)-methyl 2-(2-bromo-3-methoxy-5-methylbenzylidene)-6-methylhept-5-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1134789-25-5
Methyl 2-(dimethoxyphosphoryl)-6-methylhept-5-enoate

: 202195-05-9
2-bromo-3-methoxy-5-methylbenzaldehyde

: C₁₈H₂₃BrO₃

: 1134789-26-6
(E)-methyl 2-(2-bromo-3-methoxy-5-methylbenzylidene)-6-methylhept-5-enoate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride; In acetonitrile; at 20 ℃; for 12h; optical yield given as %de; Inert atmosphere; Large scale reaction;
DOI:10.3987/COM-08-S(F)9

Reference yield: 99.0%

: 1134789-26-6
(E)-methyl 2-(2-bromo-3-methoxy-5-methylbenzylidene)-6-methylhept-5-enoate

: 60933-65-5
(R)-S-methyl-S-phenylsulfoximine

: 1134789-27-7
C₂₅H₃₁NO₄S

Guidance literature:: With palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In toluene; at 110 - 115 ℃; for 50h; Inert atmosphere;
DOI:10.3987/COM-08-S(F)9