Technology Process of C16H12Cl5F3N4O2S
There total 6 articles about C16H12Cl5F3N4O2S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dihydrogen peroxide; trifluoroacetic acid;
In
dichloromethane;
at 12 - 15 ℃;
for 3h;
DOI:10.1021/jf1001793
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 2 h / Reflux
2: dihydrogen peroxide; trifluoroacetic acid / dichloromethane / 3 h / 12 - 15 °C
With
dihydrogen peroxide; trifluoroacetic acid;
In
dichloromethane;
DOI:10.1021/jf1001793
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sulfuric acid; sodium nitrite / acetic acid / 0.67 h / 55 - 60 °C
1.2: 5 - 20 °C
1.3: 20 °C
2.1: disulfur dichloride / dichloromethane / 20 °C
3.1: dipotassium hydrogenphosphate; sodium dithionite / water; N,N-dimethyl-formamide / 4 h / 20 °C
4.1: 36 h / Reflux; Molecular sieve
5.1: 2 h / Reflux
6.1: dihydrogen peroxide; trifluoroacetic acid / dichloromethane / 3 h / 12 - 15 °C
With
disulfur dichloride; dipotassium hydrogenphosphate; sodium dithionite; sulfuric acid; dihydrogen peroxide; trifluoroacetic acid; sodium nitrite;
In
dichloromethane; water; acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/jf1001793
