24279-39-8Relevant articles and documents
New synthesis method of 2,6-dichloro-4-trifluoromethylaniline
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Paragraph 0017; 0019-0028, (2020/01/25)
The invention discloses a new synthesis method of 2,6-dichloro-4-trifluoromethylaniline, wherein p-trifluoromethylaniline is usedas a raw material, and is added with a certain amount of sulfonyl chloride in a dropwise manner, and chlorination, water washing and pressure reducing rectification are performed to obtain the target compound. Compared with the method in the prior art, the method of theinvention has characteristics of simple process, easy operation, short reaction time, high yield and low production cost, is suitable for industrial production, is an environmentally-friendly chemicalprocess, and has good industrial application prospect.
A process for preparing 3, 4, 5 - toluene azeotrope by-product of the 2, 4, 5 - method for comprehensive utilization of toluene azeotrope (by machine translation)
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Paragraph 0014, (2017/07/19)
A process for preparing 3, 4, 5 - toluene azeotrope by-product of the 2, 4, 5 - method for comprehensive utilization of toluene azeotrope, which belongs to the field of chemical synthesis. In order to 2, 4, 5 - trifluoro toluene as the raw materials, the aminolysis reaction, catalytic hydrogenation dechlorination reaction, the chlorination reaction to synthesize 2, 6 - dichloro - 4 - trifluoromethyl aniline. The above-mentioned integrated utilization method, the useless by-product into higher economic value products, the overall yield 61.7%, purity of 99.5% or more, less impurity species, product quality and stable performance. (by machine translation)
2,6-dichloro-4-trifluoromethyl phenylamine chlorine flow production process
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Paragraph 0019-0025, (2017/09/08)
The invention relates to a 2,6-dichloro-4-trifluoromethyl phenylamine chlorine flow production process. According to the method, 2-chloro-4-trifluoromethyl-N,N-dimethylaniline is used as raw materials; 2,6-dichloro-4-trifluoromethyl phenylamine is directly prepared through chlorine gas chlorination. The technological process is simple; the single reaction quantity is increased and is twice of the original quantity; the reaction is mild; side reactions are few; the operation is simple and easy to control; the conversion rate is high; the content reaches 80 percent; chlorine gas is absorbed to obtain HCl for other production; the environment pollution cannot be caused; the environment-friendly effect is good.