3-methoxybenzoic acid anhydride

Base Information

Chemical Name:3-methoxybenzoic acid anhydride
CAS No.:94611-94-6
Molecular Formula:C₁₆H₁₄O₅
Molecular Weight:286.284
Hs Code.:

Synonyms:3-methoxybenzoic acid anhydride

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Chemical Property of 3-methoxybenzoic acid anhydride

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Technology Process of 3-methoxybenzoic acid anhydride

There total 8 articles about 3-methoxybenzoic acid anhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 74525-40-9
potassium 3-methoxybenzoate

: 1711-05-3
m-anisoyl chloride

: 94611-94-6
3-methoxybenzoic acid anhydride

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; for 0.0833333h;
DOI:10.1081/SCC-120001504

Reference yield: 98.0%

: 586-38-9
3-Methoxybenzoic acid

: 94611-94-6
3-methoxybenzoic acid anhydride

Guidance literature:: With methanesulfonyl chloride; triethylamine; In tetrahydrofuran; at 0 ℃; for 1h; Inert atmosphere;
DOI:10.1039/c8ob00178b

Reference yield: 95.0%

: 766-85-8
3-methoxy-1-iodobenzene

: 201230-82-2
carbon monoxide

: 94611-94-6
3-methoxybenzoic acid anhydride

Guidance literature:: With 1,3-bis-(diphenylphosphino)propane; water; palladium diacetate; triethylamine; In N,N-dimethyl-formamide; at 20 - 115 ℃; for 6h; under 760.051 Torr; Inert atmosphere; Autoclave;
DOI:10.1039/c2cc16611a