(R)-3-(3,4,5-trimethoxyphenyl)-1-O-benzoyl-2-O-(4-allyl-2,6-dimethoxyphenyl)-1,2-propanediol

Base Information

Chemical Name:(R)-3-(3,4,5-trimethoxyphenyl)-1-O-benzoyl-2-O-(4-allyl-2,6-dimethoxyphenyl)-1,2-propanediol
CAS No.:638168-44-2
Molecular Formula:C₃₀H₃₄O₈
Molecular Weight:522.595
Hs Code.:

Synonyms:(R)-3-(3,4,5-trimethoxyphenyl)-1-O-benzoyl-2-O-(4-allyl-2,6-dimethoxyphenyl)-1,2-propanediol

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Chemical Property of (R)-3-(3,4,5-trimethoxyphenyl)-1-O-benzoyl-2-O-(4-allyl-2,6-dimethoxyphenyl)-1,2-propanediol

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Technology Process of (R)-3-(3,4,5-trimethoxyphenyl)-1-O-benzoyl-2-O-(4-allyl-2,6-dimethoxyphenyl)-1,2-propanediol

There total 6 articles about (R)-3-(3,4,5-trimethoxyphenyl)-1-O-benzoyl-2-O-(4-allyl-2,6-dimethoxyphenyl)-1,2-propanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 6627-88-9
4-allyl-2,6-dimethoxyphenol

: 638168-43-1
(S)-3-(3,4,5-trimethoxyphenyl)-1-O-benzoyl-1,2-propanediol

: 638168-44-2
(R)-3-(3,4,5-trimethoxyphenyl)-1-O-benzoyl-2-O-(4-allyl-2,6-dimethoxyphenyl)-1,2-propanediol

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 20 ℃;

Reference yield:

: 91-10-1
1,3-dimethoxy-2-hydroxy-benzene

: 638168-44-2
(R)-3-(3,4,5-trimethoxyphenyl)-1-O-benzoyl-2-O-(4-allyl-2,6-dimethoxyphenyl)-1,2-propanediol

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / K₂CO₃ / acetone / 24 h / 20 °C

2: 92 percent / 2 h / 200 °C

3: DIAD; PPh₃ / tetrahydrofuran / 24 h / 20 °C

With di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine; In tetrahydrofuran; acetone; 2: Claisen rearrangement / 3: Mitsunobu reaction;
DOI:10.1002/jccs.200400144

Reference yield:

: 5438-54-0
1,3-dimethoxy-2-[(prop-2-en-1-yl)oxy]benzene

: 638168-44-2
(R)-3-(3,4,5-trimethoxyphenyl)-1-O-benzoyl-2-O-(4-allyl-2,6-dimethoxyphenyl)-1,2-propanediol

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / 2 h / 200 °C

2: DIAD; PPh₃ / tetrahydrofuran / 24 h / 20 °C

With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; 1: Claisen rearrangement / 2: Mitsunobu reaction;
DOI:10.1002/jccs.200400144