N-((1E)-3-(phenylimino)prop-1-enyl)benzenamine hydrochloride

Base Information

Chemical Name:N-((1E)-3-(phenylimino)prop-1-enyl)benzenamine hydrochloride
CAS No.:873293-47-1
Molecular Formula:C₁₅H₁₄N₂
Molecular Weight:222.29
Hs Code.:

Synonyms:N-((1E)-3-(phenylimino)prop-1-enyl)benzenamine hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-((1E)-3-(phenylimino)prop-1-enyl)benzenamine hydrochloride

Chemical Property:

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Technology Process of N-((1E)-3-(phenylimino)prop-1-enyl)benzenamine hydrochloride

There total 1 articles about N-((1E)-3-(phenylimino)prop-1-enyl)benzenamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 102-52-3
malonaldehydebis(dimethylacetal)

: 62-53-3
aniline

: 873293-47-1
N-((1E)-3-(phenylimino)prop-1-enyl)benzenamine hydrochloride

Guidance literature:: With hydrogenchloride; In water; at 50 ℃; for 4h;
DOI:10.1016/j.tet.2011.11.041

Reference yield: 13.0%

: 873293-47-1
N-((1E)-3-(phenylimino)prop-1-enyl)benzenamine hydrochloride

: 25299-39-2
3-anilino-propenal

: 62-53-3
aniline

Guidance literature:: With water; sodium acetate; acetic acid; In ethanol; at 70 ℃; for 33h;
DOI:10.1248/cpb.28.2356

Reference yield:

: 873293-47-1
N-((1E)-3-(phenylimino)prop-1-enyl)benzenamine hydrochloride

: C₄₀H₄₆N₅O₃S⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic anhydride / 0.5 h / Reflux; Inert atmosphere

1.2: 15 h / 20 °C / Inert atmosphere

2.1: copper(II) sulfate; L-ascorbic acid sodium salt / water; tetrahydrofuran; tert-butyl alcohol / 6 h / 20 °C

With L-ascorbic acid sodium salt; copper(II) sulfate; In tetrahydrofuran; water; acetic anhydride; tert-butyl alcohol;