Ti(CH(C(CH₃)NC₆H₃(CH(CH₃)2)2)2)(HNC₆H₃(CH(CH₃)2)2)2⁽¹⁺⁾*B(C₆F₅)4^(1-)=Ti(CH(C(CH₃)NC₆H₃(C₃H₇)2)2)(HNC₆H₃(C₃H₇)2)2B(C₆F₅)4

Base Information

• Chemical Name: Ti(CH(C(CH₃)NC₆H₃(CH(CH₃)2)2)2)(HNC₆H₃(CH(CH₃)2)2)2⁽¹⁺⁾*B(C₆F₅)4^(1-)=Ti(CH(C(CH₃)NC₆H₃(C₃H₇)2)2)(HNC₆H₃(C₃H₇)2)2B(C₆F₅)4
• CAS No.: 624733-38-6
• Molecular Formula: C₂₄BF₂₀*C₅₃H₇₇N₄Ti
• Molecular Weight: 1497.14

Synonyms:Ti(CH(C(CH₃)NC₆H₃(CH(CH₃)2)2)2)(HNC₆H₃(CH(CH₃)2)2)2⁽¹⁺⁾*B(C₆F₅)4^(1-)=Ti(CH(C(CH₃)NC₆H₃(C₃H₇)2)2)(HNC₆H₃(C₃H₇)2)2B(C₆F₅)4

Chemical Property of Ti(CH(C(CH₃)NC₆H₃(CH(CH₃)2)2)2)(HNC₆H₃(CH(CH₃)2)2)2⁽¹⁺⁾*B(C₆F₅)4^(1-)=Ti(CH(C(CH₃)NC₆H₃(C₃H₇)2)2)(HNC₆H₃(C₃H₇)2)2B(C₆F₅)4

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Technology Process of Ti(CH(C(CH₃)NC₆H₃(CH(CH₃)2)2)2)(HNC₆H₃(CH(CH₃)2)2)2⁽¹⁺⁾*B(C₆F₅)4^(1-)=Ti(CH(C(CH₃)NC₆H₃(C₃H₇)2)2)(HNC₆H₃(C₃H₇)2)2B(C₆F₅)4

There total 1 articles about Ti(CH(C(CH₃)NC₆H₃(CH(CH₃)2)2)2)(HNC₆H₃(CH(CH₃)2)2)2⁽¹⁺⁾*B(C₆F₅)4^(1-)=Ti(CH(C(CH₃)NC₆H₃(C₃H₇)2)2)(HNC₆H₃(C₃H₇)2)2B(C₆F₅)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

Ti(CH(C(CH3)NC6H3(CH(CH3)2)2)2)(HNC6H3(CH(CH3)2)2)2(1+)*O3SCF3(1-)=[Ti(CH(C(CH3)NC6H3(C3H7)2)2)(HNC6H3(C3H7)2)2]O3SCF3 (623924-16-3) + decamethylferrocenium tetrakis(pentafluorophenyl)borate (135348-60-6) → Ti(CH(C(CH3)NC6H3(CH(CH3)2)2)2)(HNC6H3(CH(CH3)2)2)2(1+)*B(C6F5)4(1-)=Ti(CH(C(CH3)NC6H3(C3H7)2)2)(HNC6H3(C3H7)2)2B(C6F5)4 (624733-38-6)

Guidance literature:

In diethyl ether; byproducts: (C5(CH3)5)2Fe; at -35°C;

DOI:10.1039/b304633h

Reference yield:

Ti(CH(C(CH3)NC6H3(CH(CH3)2)2)2)(HNC6H3(CH(CH3)2)2)2(1+)*B(C6F5)4(1-)=Ti(CH(C(CH3)NC6H3(C3H7)2)2)(HNC6H3(C3H7)2)2B(C6F5)4 (624733-38-6) + thallium(I) triflate (73491-36-8) → ((2,6-[CH(CH3)2]2C6H3)NC(CH3)CHC(CH3)N(2,6-[CH(CH3)2]2C6H3))Ti=NC6H3-2,6-[CH(CH3)2]2(OTf) (623924-17-4)

Guidance literature:

In dichloromethane;

DOI:10.1039/b304633h

upstream raw materials:

Ti(CH(C(CH₃)NC₆H₃(CH(CH₃)2)2)2)(HNC₆H₃(CH(CH₃)2)2)2⁽¹⁺⁾*O₃SCF₃^(1-)=[Ti(CH(C(CH₃)NC₆H₃(C₃H₇)2)2)(HNC₆H₃(C₃H₇)2)2]O₃SCF₃

decamethylferrocenium tetrakis(pentafluorophenyl)borate

Downstream raw materials:

((2,6-[CH(CH₃)2]2C₆H₃)NC(CH₃)CHC(CH₃)N(2,6-[CH(CH₃)2]2C₆H₃))Ti=NC₆H₃-2,6-[CH(CH₃)2]2(OTf)

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