9-(4-chlorobenzoyl)-6-methoxy-2,3,4,9-tetrahydro-1H-carbazole-3-carboxylic acid

Base Information

Chemical Name:9-(4-chlorobenzoyl)-6-methoxy-2,3,4,9-tetrahydro-1H-carbazole-3-carboxylic acid
CAS No.:36405-72-8
Molecular Formula:C₂₁H₁₈ClNO₄
Molecular Weight:383.831
Hs Code.:

Synonyms:9-(4-chlorobenzoyl)-6-methoxy-2,3,4,9-tetrahydro-1H-carbazole-3-carboxylic acid

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Chemical Property of 9-(4-chlorobenzoyl)-6-methoxy-2,3,4,9-tetrahydro-1H-carbazole-3-carboxylic acid

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Technology Process of 9-(4-chlorobenzoyl)-6-methoxy-2,3,4,9-tetrahydro-1H-carbazole-3-carboxylic acid

There total 13 articles about 9-(4-chlorobenzoyl)-6-methoxy-2,3,4,9-tetrahydro-1H-carbazole-3-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 874-61-3
4-oxocyclohexanecarboxylic acid

: 13815-62-8
N¹-(4-Chlorbenzoyl)-N¹-(4-methoxyphenyl)hydrazin-hydrochlorid

: 36405-72-8
9-(4-chlorobenzoyl)-6-methoxy-2,3,4,9-tetrahydro-1H-carbazole-3-carboxylic acid

Guidance literature:: With acetic acid; In water; at 80 ℃; for 3h;
DOI:10.1021/jm3017656

Reference yield: 82.0%

: 16205-98-4
3-oxo-cyclohexanecarboxylic acid

: 13815-62-8
N¹-(4-Chlorbenzoyl)-N¹-(4-methoxyphenyl)hydrazin-hydrochlorid

: 36405-72-8
9-(4-chlorobenzoyl)-6-methoxy-2,3,4,9-tetrahydro-1H-carbazole-3-carboxylic acid

Guidance literature:: With acetic acid; In water; at 80 ℃; for 3h;
DOI:10.1021/jm3017656

Reference yield: 28.9%

: 9-(4-chlorobenzoyl)-6-hydroxy-2,3,4,9-tetrahydro-1H-carbazole-3-carboxylic acid

: 74-88-4
methyl iodide

: 36405-72-8
9-(4-chlorobenzoyl)-6-methoxy-2,3,4,9-tetrahydro-1H-carbazole-3-carboxylic acid

Guidance literature:: 9-(4-chlorobenzoyl)-6-hydroxy-2,3,4,9-tetrahydro-1H-carbazole-3-carboxylic acid; With sodium hydride; In N,N-dimethyl-formamide; at -10 ℃; for 0.166667h; Inert atmosphere;

methyl iodide; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.ejmech.2018.02.069