3,4-dimethoxybenzoic acid 4-bromobutyl ester

Base Information

Chemical Name:3,4-dimethoxybenzoic acid 4-bromobutyl ester
CAS No.:1260668-38-9
Molecular Formula:C₁₃H₁₇BrO₄
Molecular Weight:317.18
Hs Code.:

Synonyms:3,4-dimethoxybenzoic acid 4-bromobutyl ester

Suppliers and Price of 3,4-dimethoxybenzoic acid 4-bromobutyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 5 raw suppliers

Chemical Property of 3,4-dimethoxybenzoic acid 4-bromobutyl ester

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of 3,4-dimethoxybenzoic acid 4-bromobutyl ester

There total 1 articles about 3,4-dimethoxybenzoic acid 4-bromobutyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110-52-1
1,4-dibromo-butane

: 93-07-2
Veratric acid

: 1260668-38-9
3,4-dimethoxybenzoic acid 4-bromobutyl ester

Guidance literature:: With potassium carbonate; In acetone; at 65 ℃; for 20h;
DOI:10.1016/j.bmc.2012.11.044

Reference yield:

: 1260668-38-9
3,4-dimethoxybenzoic acid 4-bromobutyl ester

: 286381-74-6
(S)-2-benzyloxy-5,6,7,8-tetrahydro-quinolin-5-ylamine

: C₂₉H₃₆N₂O₅

Guidance literature:: In toluene; for 20h; Reflux;
DOI:10.1016/j.bmc.2012.11.044

Reference yield:

: 1260668-38-9
3,4-dimethoxybenzoic acid 4-bromobutyl ester

: 1421022-14-1
(S)-3,4-dimethoxybenzoic acid 4-(2-oxo-1,2,5,6,7,8-hexahydroquinolin-5-ylamino)butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 20 h / Reflux

2: palladium 10% on activated carbon; hydrogen / methanol / 3 h / 20 °C

With palladium 10% on activated carbon; hydrogen; In methanol; toluene;
DOI:10.1016/j.bmc.2012.11.044