(S)-3,4-dimethoxybenzoic acid 4-(2-oxo-1,2,5,6,7,8-hexahydroquinolin-5-ylamino)butyl ester

Base Information

Chemical Name:(S)-3,4-dimethoxybenzoic acid 4-(2-oxo-1,2,5,6,7,8-hexahydroquinolin-5-ylamino)butyl ester
CAS No.:1421022-14-1
Molecular Formula:C₂₂H₂₈N₂O₅
Molecular Weight:400.475
Hs Code.:

Synonyms:(S)-3,4-dimethoxybenzoic acid 4-(2-oxo-1,2,5,6,7,8-hexahydroquinolin-5-ylamino)butyl ester

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Chemical Property of (S)-3,4-dimethoxybenzoic acid 4-(2-oxo-1,2,5,6,7,8-hexahydroquinolin-5-ylamino)butyl ester

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Technology Process of (S)-3,4-dimethoxybenzoic acid 4-(2-oxo-1,2,5,6,7,8-hexahydroquinolin-5-ylamino)butyl ester

There total 3 articles about (S)-3,4-dimethoxybenzoic acid 4-(2-oxo-1,2,5,6,7,8-hexahydroquinolin-5-ylamino)butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₉H₃₆N₂O₅

: 1421022-14-1
(S)-3,4-dimethoxybenzoic acid 4-(2-oxo-1,2,5,6,7,8-hexahydroquinolin-5-ylamino)butyl ester

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃; for 3h;
DOI:10.1016/j.bmc.2012.11.044

Reference yield:

: 1260668-38-9
3,4-dimethoxybenzoic acid 4-bromobutyl ester

: 1421022-14-1
(S)-3,4-dimethoxybenzoic acid 4-(2-oxo-1,2,5,6,7,8-hexahydroquinolin-5-ylamino)butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 20 h / Reflux

2: palladium 10% on activated carbon; hydrogen / methanol / 3 h / 20 °C

With palladium 10% on activated carbon; hydrogen; In methanol; toluene;
DOI:10.1016/j.bmc.2012.11.044

Reference yield:

: 93-07-2
Veratric acid

: 1421022-14-1
(S)-3,4-dimethoxybenzoic acid 4-(2-oxo-1,2,5,6,7,8-hexahydroquinolin-5-ylamino)butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetone / 20 h / 65 °C

2: toluene / 20 h / Reflux

3: palladium 10% on activated carbon; hydrogen / methanol / 3 h / 20 °C

With palladium 10% on activated carbon; hydrogen; potassium carbonate; In methanol; acetone; toluene;
DOI:10.1016/j.bmc.2012.11.044