1,10a-dihydropyrrolo[1,2-b]isoquinoline-3,10(2H,5H)-dione 10-(O-benzyloxime)

Base Information

Chemical Name:1,10a-dihydropyrrolo[1,2-b]isoquinoline-3,10(2H,5H)-dione 10-(O-benzyloxime)
CAS No.:1384106-02-8
Molecular Formula:C₁₉H₁₈N₂O₂
Molecular Weight:306.364
Hs Code.:

Synonyms:1,10a-dihydropyrrolo[1,2-b]isoquinoline-3,10(2H,5H)-dione 10-(O-benzyloxime)

Suppliers and Price of 1,10a-dihydropyrrolo[1,2-b]isoquinoline-3,10(2H,5H)-dione 10-(O-benzyloxime)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1,10a-dihydropyrrolo[1,2-b]isoquinoline-3,10(2H,5H)-dione 10-(O-benzyloxime)

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,10a-dihydropyrrolo[1,2-b]isoquinoline-3,10(2H,5H)-dione 10-(O-benzyloxime)

There total 2 articles about 1,10a-dihydropyrrolo[1,2-b]isoquinoline-3,10(2H,5H)-dione 10-(O-benzyloxime) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 106351-35-3
1,10a-dihydropyrrolo[1,2-b]isoquinoline-3,10(2H,5H)-dione 10-oxime

: 100-39-0
benzyl bromide

: 1384106-02-8
1,10a-dihydropyrrolo[1,2-b]isoquinoline-3,10(2H,5H)-dione 10-(O-benzyloxime)

Guidance literature:: With tetra-(n-butyl)ammonium hydrogensulfate; sodium hydroxide; In dichloromethane; water; for 12h; Reflux;
DOI:10.1016/j.tet.2012.04.056

Reference yield:

: 103201-08-7
1,2,3,5,10,10a-hexahydropyrrolo[1,2-b]isoquinolin-3,10dione

: 1384106-02-8
1,10a-dihydropyrrolo[1,2-b]isoquinoline-3,10(2H,5H)-dione 10-(O-benzyloxime)

Guidance literature:: Multi-step reaction with 2 steps

1: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 5 h / Reflux

2: tetra-(n-butyl)ammonium hydrogensulfate; sodium hydroxide / dichloromethane; water / 12 h / Reflux

With tetra-(n-butyl)ammonium hydrogensulfate; hydroxylamine hydrochloride; sodium acetate; sodium hydroxide; In ethanol; dichloromethane; water;
DOI:10.1016/j.tet.2012.04.056