(E)-1-<4-<<3-aza-8-(chloroacetamido)-3-(chloroacetyl)octamethylene>oxy>phenyl>-2-chloro-1,2-diphenylethylene

Base Information

Chemical Name:(E)-1-<4-<<3-aza-8-(chloroacetamido)-3-(chloroacetyl)octamethylene>oxy>phenyl>-2-chloro-1,2-diphenylethylene
CAS No.:95764-39-9
Molecular Formula:C₃₁H₃₃Cl₃N₂O₃
Molecular Weight:587.974
Hs Code.:

Synonyms:(E)-1-<4-<<3-aza-8-(chloroacetamido)-3-(chloroacetyl)octamethylene>oxy>phenyl>-2-chloro-1,2-diphenylethylene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-1-<4-<<3-aza-8-(chloroacetamido)-3-(chloroacetyl)octamethylene>oxy>phenyl>-2-chloro-1,2-diphenylethylene

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Technology Process of (E)-1-<4-<<3-aza-8-(chloroacetamido)-3-(chloroacetyl)octamethylene>oxy>phenyl>-2-chloro-1,2-diphenylethylene

There total 7 articles about (E)-1-<4-<<3-aza-8-(chloroacetamido)-3-(chloroacetyl)octamethylene>oxy>phenyl>-2-chloro-1,2-diphenylethylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 95764-38-8
(E)-1-<4-<(8-amino-3-azaoctamethylene)oxy>phenyl>-2-chloro-1,2-diphenylethylene dihydrobromide

: 79-04-9
chloroacetyl chloride

: 95764-39-9
(E)-1-<4-<<3-aza-8-(chloroacetamido)-3-(chloroacetyl)octamethylene>oxy>phenyl>-2-chloro-1,2-diphenylethylene

Guidance literature:: With sodium hydroxide; In 1,2-dichloro-ethane; for 3h;
DOI:10.1021/jm00383a010

Reference yield:

: 38459-64-2
(4-(2-bromoethoxy)phenyl)(phenyl)methanone

: 95764-39-9
(E)-1-<4-<<3-aza-8-(chloroacetamido)-3-(chloroacetyl)octamethylene>oxy>phenyl>-2-chloro-1,2-diphenylethylene

Guidance literature:: Multi-step reaction with 6 steps

1: diethyl ether; benzene / 1.5 h / Heating

2: 100 percent / 7.8 N HCl / ethanol / 7 h / Heating

3: 64 percent / Cl₂ / CCl₄ / 2.5 h / Heating

4: 75 percent / pentan-1-ol / 5 h / Ambient temperature

5: 82 percent / HBr / acetic acid / 1.5 h

6: 46 percent / 0.5 N aq. NaOH / 1,2-dichloro-ethane / 3 h

With hydrogenchloride; sodium hydroxide; hydrogen bromide; chlorine; In tetrachloromethane; diethyl ether; ethanol; pentan-1-ol; acetic acid; 1,2-dichloro-ethane; benzene;
DOI:10.1021/jm00383a010

Reference yield:

: 95764-34-4,95764-35-5
(Z/E)-1-<4-(2-bromoethoxy)phenyl>-1,2-diphenyl ethene

: 95764-39-9
(E)-1-<4-<<3-aza-8-(chloroacetamido)-3-(chloroacetyl)octamethylene>oxy>phenyl>-2-chloro-1,2-diphenylethylene

Guidance literature:: Multi-step reaction with 4 steps

1: 64 percent / Cl₂ / CCl₄ / 2.5 h / Heating

2: 75 percent / pentan-1-ol / 5 h / Ambient temperature

3: 82 percent / HBr / acetic acid / 1.5 h

4: 46 percent / 0.5 N aq. NaOH / 1,2-dichloro-ethane / 3 h

With sodium hydroxide; hydrogen bromide; chlorine; In tetrachloromethane; pentan-1-ol; acetic acid; 1,2-dichloro-ethane;
DOI:10.1021/jm00383a010