N-{(S)-(5'-tert-butoxycarbonyl-2'-methylphenyl)[(-)-8-phenylmenthyloxycarbonyl]methyl}-N-(4''-cyanobenzyl)-N,N-dimethylammonium bromide

Base Information

Chemical Name:N-{(S)-(5'-tert-butoxycarbonyl-2'-methylphenyl)[(-)-8-phenylmenthyloxycarbonyl]methyl}-N-(4''-cyanobenzyl)-N,N-dimethylammonium bromide
CAS No.:1088481-76-8
Molecular Formula:Br*C₄₀H₅₁N₂O₄
Molecular Weight:703.76
Hs Code.:

Synonyms:N-{(S)-(5'-tert-butoxycarbonyl-2'-methylphenyl)[(-)-8-phenylmenthyloxycarbonyl]methyl}-N-(4''-cyanobenzyl)-N,N-dimethylammonium bromide

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Chemical Property of N-{(S)-(5'-tert-butoxycarbonyl-2'-methylphenyl)[(-)-8-phenylmenthyloxycarbonyl]methyl}-N-(4''-cyanobenzyl)-N,N-dimethylammonium bromide

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Technology Process of N-{(S)-(5'-tert-butoxycarbonyl-2'-methylphenyl)[(-)-8-phenylmenthyloxycarbonyl]methyl}-N-(4''-cyanobenzyl)-N,N-dimethylammonium bromide

There total 1 articles about N-{(S)-(5'-tert-butoxycarbonyl-2'-methylphenyl)[(-)-8-phenylmenthyloxycarbonyl]methyl}-N-(4''-cyanobenzyl)-N,N-dimethylammonium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1004759-69-6
(2S)-2-(5'-tert-butoxycarbonyl-2'-methylphenyl)-2-(dimethylamino)acetic acid (-)-8-phenylmenthol ester

: 17201-43-3
4-cyanobenzyl bromide

: 1088481-76-8
N-{(S)-(5'-tert-butoxycarbonyl-2'-methylphenyl)[(-)-8-phenylmenthyloxycarbonyl]methyl}-N-(4''-cyanobenzyl)-N,N-dimethylammonium bromide

Guidance literature:: In acetonitrile; at 20 ℃;
DOI:10.1039/b811162f

Reference yield:

: 1088481-76-8
N-{(S)-(5'-tert-butoxycarbonyl-2'-methylphenyl)[(-)-8-phenylmenthyloxycarbonyl]methyl}-N-(4''-cyanobenzyl)-N,N-dimethylammonium bromide

: 2-(5'-tert-butoxycarbonyl-2'-methylphenyl)-3-(4''-cyanophenyl)-2-dimethylaminopropionic acid (-)-8-phenylmenthol ester

: 2-(5'-tert-butoxycarbonyl-2'-methylphenyl)-3-(4''-cyanophenyl)-2-dimethylaminopropionic acid (-)-8-phenylmenthol ester

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at -60 ℃; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1039/b811162f