(4S)-3-(Benzyloxy)-4-methoxy-<3-oxo-3-<2-oxo-4-(phenylmethyl)-3-oxazolidinyl>propyl>benzene

Base Information

Chemical Name:(4S)-3-(Benzyloxy)-4-methoxy-<3-oxo-3-<2-oxo-4-(phenylmethyl)-3-oxazolidinyl>propyl>benzene
CAS No.:159749-97-0
Molecular Formula:C₂₇H₂₇NO₅
Molecular Weight:445.515
Hs Code.:

Synonyms:(4S)-3-(Benzyloxy)-4-methoxy-<3-oxo-3-<2-oxo-4-(phenylmethyl)-3-oxazolidinyl>propyl>benzene

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Chemical Property of (4S)-3-(Benzyloxy)-4-methoxy-<3-oxo-3-<2-oxo-4-(phenylmethyl)-3-oxazolidinyl>propyl>benzene

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Technology Process of (4S)-3-(Benzyloxy)-4-methoxy-<3-oxo-3-<2-oxo-4-(phenylmethyl)-3-oxazolidinyl>propyl>benzene

There total 6 articles about (4S)-3-(Benzyloxy)-4-methoxy-<3-oxo-3-<2-oxo-4-(phenylmethyl)-3-oxazolidinyl>propyl>benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 621-59-0
isovanillin

: 159749-97-0
(4S)-3-(Benzyloxy)-4-methoxy-<3-oxo-3-<2-oxo-4-(phenylmethyl)-3-oxazolidinyl>propyl>benzene

Guidance literature:: Multi-step reaction with 6 steps

1: 86 percent / piperidine / pyridine / 1.) 105 deg C, 3 h, 2.) 145 deg C, 1 h

2: 88 percent / H₂ / 10percent Pd-C / methanol / 12 h / Ambient temperature

3: 89 percent / K₂CO₃ / acetone / 20 h / Heating

4: 96 percent / aq. KOH / methanol; tetrahydrofuran / 2 h / Ambient temperature

5: Et₃N / tetrahydrofuran / 1.) -78 deg C, 15 min, 2.) room temp., 50 min

6: n-BuLi / 1.) THF, hexane, -78 deg C, 20 min, 2.) -78 deg C, 15 min and room temp., 4 h

With piperidine; potassium hydroxide; n-butyllithium; hydrogen; potassium carbonate; triethylamine; palladium on activated charcoal; In tetrahydrofuran; pyridine; methanol; acetone;
DOI:10.1021/jo00088a009

Reference yield:

: 537-73-5,1135-16-6,25522-33-2
isoferulic acid

: 159749-97-0
(4S)-3-(Benzyloxy)-4-methoxy-<3-oxo-3-<2-oxo-4-(phenylmethyl)-3-oxazolidinyl>propyl>benzene

Guidance literature:: Multi-step reaction with 5 steps

1: 88 percent / H₂ / 10percent Pd-C / methanol / 12 h / Ambient temperature

2: 89 percent / K₂CO₃ / acetone / 20 h / Heating

3: 96 percent / aq. KOH / methanol; tetrahydrofuran / 2 h / Ambient temperature

4: Et₃N / tetrahydrofuran / 1.) -78 deg C, 15 min, 2.) room temp., 50 min

5: n-BuLi / 1.) THF, hexane, -78 deg C, 20 min, 2.) -78 deg C, 15 min and room temp., 4 h

With potassium hydroxide; n-butyllithium; hydrogen; potassium carbonate; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; acetone;
DOI:10.1021/jo00088a009

Reference yield:

: 36418-96-9
3-<3-(Benzyloxy)-4-methoxyphenyl>propionic acid

: 159749-97-0
(4S)-3-(Benzyloxy)-4-methoxy-<3-oxo-3-<2-oxo-4-(phenylmethyl)-3-oxazolidinyl>propyl>benzene

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / tetrahydrofuran / 1.) -78 deg C, 15 min, 2.) room temp., 50 min

2: n-BuLi / 1.) THF, hexane, -78 deg C, 20 min, 2.) -78 deg C, 15 min and room temp., 4 h

With n-butyllithium; triethylamine; In tetrahydrofuran;
DOI:10.1021/jo00088a009