O-dibenzylisolariciresinol

Base Information

Chemical Name:O-dibenzylisolariciresinol
CAS No.:111266-05-8
Molecular Formula:C₃₄H₃₆O₆
Molecular Weight:540.656
Hs Code.:

Synonyms:O-dibenzylisolariciresinol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O-dibenzylisolariciresinol

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Technology Process of O-dibenzylisolariciresinol

There total 6 articles about O-dibenzylisolariciresinol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 111194-10-6
O-dibenzylretrodendrin

: 111266-05-8
O-dibenzylisolariciresinol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 1h; Ambient temperature;
DOI:10.3987/R-1987-05-1169

Reference yield:

: 2426-87-1
3-methoxy-4-(phenylmethoxy)benzaldehyde

: 111266-05-8
O-dibenzylisolariciresinol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) lithium hexamethyldisilylamide (LHDS) / 1.) benzene, 2.) benzene, 0 deg C, 5 min

2: 78 percent / 60percent aq. perchloric acid / acetic acid; CH₂Cl₂ / 4.5 h / Ambient temperature

3: 80 percent / LiAlH₄ / tetrahydrofuran / 1 h / Ambient temperature

With lithium aluminium tetrahydride; perchloric acid; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; acetic acid;
DOI:10.3987/R-1987-05-1169

Reference yield:

: 111266-03-6
(R)-(+)-3-(4-benzyloxy-3-methoxybenzyl)-γ-butyrolactone

: 111266-05-8
O-dibenzylisolariciresinol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) lithium hexamethyldisilylamide (LHDS) / 1.) benzene, 2.) benzene, 0 deg C, 5 min

2: 78 percent / 60percent aq. perchloric acid / acetic acid; CH₂Cl₂ / 4.5 h / Ambient temperature

3: 80 percent / LiAlH₄ / tetrahydrofuran / 1 h / Ambient temperature

With lithium aluminium tetrahydride; perchloric acid; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; acetic acid;
DOI:10.3987/R-1987-05-1169