4,4,4-trifluorobutyl cyclohex-1-enecarboxylate

Base Information

Chemical Name:4,4,4-trifluorobutyl cyclohex-1-enecarboxylate
CAS No.:1449522-66-0
Molecular Formula:C₁₁H₁₅F₃O₂
Molecular Weight:236.234
Hs Code.:

Synonyms:4,4,4-trifluorobutyl cyclohex-1-enecarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,4,4-trifluorobutyl cyclohex-1-enecarboxylate

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Technology Process of 4,4,4-trifluorobutyl cyclohex-1-enecarboxylate

There total 1 articles about 4,4,4-trifluorobutyl cyclohex-1-enecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 461-18-7
4,4,4-trifluorobutanol

: 636-82-8
cyclohexene-1-carboxylic acid

: 1449522-66-0
4,4,4-trifluorobutyl cyclohex-1-enecarboxylate

Guidance literature:: With dmap; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1039/c3cc44149k

Reference yield:

: 1449522-66-0
4,4,4-trifluorobutyl cyclohex-1-enecarboxylate

: 73183-34-3
bis(pinacol)diborane

: 1449522-56-8
4,4,4-trifluorobutyl 2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)cyclohex-1-enecarboxylate

Guidance literature:: bis(pinacol)diborane; With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; triphenyl-arsane; In octane; at 20 ℃; for 0.166667h; Inert atmosphere;

4,4,4-trifluorobutyl cyclohex-1-enecarboxylate; In octane; at 120 ℃; for 3h; chemoselective reaction; Inert atmosphere;
DOI:10.1039/c3cc44149k