1,5-diacetamido-2,4-dipyrrolidinobenzene

Base Information

Chemical Name:1,5-diacetamido-2,4-dipyrrolidinobenzene
CAS No.:261375-29-5
Molecular Formula:C₁₈H₂₆N₄O₂
Molecular Weight:330.43
Hs Code.:

Synonyms:1,5-diacetamido-2,4-dipyrrolidinobenzene

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Chemical Property of 1,5-diacetamido-2,4-dipyrrolidinobenzene

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Technology Process of 1,5-diacetamido-2,4-dipyrrolidinobenzene

There total 3 articles about 1,5-diacetamido-2,4-dipyrrolidinobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 108-24-7
acetic anhydride

: 4,6-di-pyrrolidin-1-yl-benzene-1,3-diamine

: 261375-29-5
1,5-diacetamido-2,4-dipyrrolidinobenzene

Guidance literature:: With acetic acid; at 20 ℃; for 1.5h;
DOI:10.1021/jm990210q

Reference yield:

: 24239-82-5
1,5-dibromo-2,4-dinitrobenzene

: 261375-29-5
1,5-diacetamido-2,4-dipyrrolidinobenzene

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / 12 h / 90 °C

2: H₂; AcOH / 5percent Pd/C / 12 h / 2585.81 Torr

3: 88 percent / AcOH / 1.5 h / 20 °C

With hydrogen; acetic acid; 5percent Pd/C; 1: Substitution / 2: Reduction / 3: Acetylation;
DOI:10.1021/jm990210q

Reference yield:

: 261375-28-4
C₁₄H₁₈N₄O₄

: 261375-29-5
1,5-diacetamido-2,4-dipyrrolidinobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: H₂; AcOH / 5percent Pd/C / 12 h / 2585.81 Torr

2: 88 percent / AcOH / 1.5 h / 20 °C

With hydrogen; acetic acid; 5percent Pd/C; 1: Reduction / 2: Acetylation;
DOI:10.1021/jm990210q