(5S)-1-(tert-butoxycarbonyl)-5-{(R)-trimethylsilanyloxy[(R)-(2,2-dimethyl-1,3-dioxolan-4-yl)](phenyl)methyl}-1H-pyrrol-2(5H)-one

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Chemical Name:(5S)-1-(tert-butoxycarbonyl)-5-{(R)-trimethylsilanyloxy[(R)-(2,2-dimethyl-1,3-dioxolan-4-yl)](phenyl)methyl}-1H-pyrrol-2(5H)-one
CAS No.:1034170-12-1
Molecular Formula:C₂₄H₃₅NO₆Si
Molecular Weight:461.631
Hs Code.:

Synonyms:(5S)-1-(tert-butoxycarbonyl)-5-{(R)-trimethylsilanyloxy[(R)-(2,2-dimethyl-1,3-dioxolan-4-yl)](phenyl)methyl}-1H-pyrrol-2(5H)-one

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Chemical Property of (5S)-1-(tert-butoxycarbonyl)-5-{(R)-trimethylsilanyloxy[(R)-(2,2-dimethyl-1,3-dioxolan-4-yl)](phenyl)methyl}-1H-pyrrol-2(5H)-one

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Technology Process of (5S)-1-(tert-butoxycarbonyl)-5-{(R)-trimethylsilanyloxy[(R)-(2,2-dimethyl-1,3-dioxolan-4-yl)](phenyl)methyl}-1H-pyrrol-2(5H)-one

There total 2 articles about (5S)-1-(tert-butoxycarbonyl)-5-{(R)-trimethylsilanyloxy[(R)-(2,2-dimethyl-1,3-dioxolan-4-yl)](phenyl)methyl}-1H-pyrrol-2(5H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 27607-77-8
trimethylsilyl trifluoromethanesulfonate

: 141293-14-3
N-(tert-butoxycarbonyl)pyrrol-2(5H)-one

: 16354-97-5
[(R)-2,2-dimethyl-1,3-dioxolan-4-yl]phenylmethanone

: 1034170-12-1
(5S)-1-(tert-butoxycarbonyl)-5-{(R)-trimethylsilanyloxy[(R)-(2,2-dimethyl-1,3-dioxolan-4-yl)](phenyl)methyl}-1H-pyrrol-2(5H)-one

Guidance literature:: With triethylamine; In diethyl ether; dichloromethane; at -78 ℃; for 24h;
DOI:10.1021/jo800741c

Reference yield:

: 27607-77-8
trimethylsilyl trifluoromethanesulfonate

: 141293-28-9
N-(tert-butoxycarbonyl)-2-[(tert-butyldimethylsilyl)oxy]pyrrole

: 16354-97-5
[(R)-2,2-dimethyl-1,3-dioxolan-4-yl]phenylmethanone

: 1034170-12-1
(5S)-1-(tert-butoxycarbonyl)-5-{(R)-trimethylsilanyloxy[(R)-(2,2-dimethyl-1,3-dioxolan-4-yl)](phenyl)methyl}-1H-pyrrol-2(5H)-one

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at -80 ℃; for 4h; diastereoselective reaction; Inert atmosphere;
DOI:10.1002/ejoc.200800040