2-bromo-4-phenoxyphenoxyethyl tetrahydropyranyl ether

Base Information

Chemical Name:2-bromo-4-phenoxyphenoxyethyl tetrahydropyranyl ether
CAS No.:205380-90-1
Molecular Formula:C₁₉H₂₁BrO₄
Molecular Weight:393.277
Hs Code.:

Synonyms:2-bromo-4-phenoxyphenoxyethyl tetrahydropyranyl ether

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Chemical Property of 2-bromo-4-phenoxyphenoxyethyl tetrahydropyranyl ether

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Technology Process of 2-bromo-4-phenoxyphenoxyethyl tetrahydropyranyl ether

There total 2 articles about 2-bromo-4-phenoxyphenoxyethyl tetrahydropyranyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 831-82-3
4-Phenoxyphenol

: 205380-90-1
2-bromo-4-phenoxyphenoxyethyl tetrahydropyranyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / t-BuNH₂, Br₂ / toluene / -70 - 20 °C

2: 1.) KOH / 1.) DMSO, RT, 5 min, 2.) DMSO, RT, overnight

With potassium hydroxide; bromine; tert-butylamine; In toluene;
DOI:10.1021/jm970860z

Reference yield:

: 17739-45-6,59146-56-4
2-(2-bromoethoxy)tetrahydropyran

: 54582-60-4
2-bromo-4-phenoxy-phenol

: 205380-90-1
2-bromo-4-phenoxyphenoxyethyl tetrahydropyranyl ether

Guidance literature:: With potassium hydroxide; Yield given. Multistep reaction; 1.) DMSO, RT, 5 min, 2.) DMSO, RT, overnight;
DOI:10.1021/jm970860z