dimethyl(4-trifluoromethylphenyl)silyl formate

Base Information

Chemical Name:dimethyl(4-trifluoromethylphenyl)silyl formate
CAS No.:1415919-37-7
Molecular Formula:C₁₀H₁₁F₃O₂Si
Molecular Weight:248.277
Hs Code.:

Synonyms:dimethyl(4-trifluoromethylphenyl)silyl formate

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Chemical Property of dimethyl(4-trifluoromethylphenyl)silyl formate

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Technology Process of dimethyl(4-trifluoromethylphenyl)silyl formate

There total 2 articles about dimethyl(4-trifluoromethylphenyl)silyl formate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 124-38-9,18923-20-1
carbon dioxide

: 19254-78-5
dimethyl(4-trifluoromethylphenyl)silane

: 1415919-37-7
dimethyl(4-trifluoromethylphenyl)silyl formate

: 1,3-bis[4′-(trifluoromethyl)phenyl]-1,1,3,3-tetramethyldisiloxane

Guidance literature:: dimethyl(4-trifluoromethylphenyl)silane; With dirhodium tetraacetate; potassium carbonate; In acetonitrile; Schlenk technique; Inert atmosphere;

carbon dioxide; In acetonitrile; at 50 ℃; for 2h; Schlenk technique;
DOI:10.1016/j.molcata.2012.10.014

Reference yield:

: 124-38-9,18923-20-1
carbon dioxide

: 19254-78-5
dimethyl(4-trifluoromethylphenyl)silane

: 1415919-37-7
dimethyl(4-trifluoromethylphenyl)silyl formate

Guidance literature:: With dirhodium tetraacetate; potassium carbonate; In acetonitrile; at 50 ℃; for 2h; under 750.075 Torr; Glovebox; Schlenk technique; Sealed tube;
DOI:10.1039/c8cc02276c

Reference yield: 68.0%

: 1415919-37-7
dimethyl(4-trifluoromethylphenyl)silyl formate

: 228873-97-0
hydroxy(dimethyl)(4-trifluoromethylphenyl)silane

Guidance literature:: With carbonylhydrido(tetrahydroborato)[bis(2-diphenylphosphinoethyl)amino]ruthenium(II); hydrogen; In tetrahydrofuran; at 150 ℃; for 12h; under 7500.75 Torr; Glovebox; Autoclave; Sealed tube;
DOI:10.1039/c8cc02276c