5-(tert-butyl-dimethyl-silanyloxy)-2-[2-(4-methoxyphenyl)-1-methyl-ethyl]-pyridine

Base Information

Chemical Name:5-(tert-butyl-dimethyl-silanyloxy)-2-[2-(4-methoxyphenyl)-1-methyl-ethyl]-pyridine
CAS No.:1187188-78-8
Molecular Formula:C₂₁H₃₁NO₂Si
Molecular Weight:357.568
Hs Code.:

Synonyms:5-(tert-butyl-dimethyl-silanyloxy)-2-[2-(4-methoxyphenyl)-1-methyl-ethyl]-pyridine

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Chemical Property of 5-(tert-butyl-dimethyl-silanyloxy)-2-[2-(4-methoxyphenyl)-1-methyl-ethyl]-pyridine

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Technology Process of 5-(tert-butyl-dimethyl-silanyloxy)-2-[2-(4-methoxyphenyl)-1-methyl-ethyl]-pyridine

There total 1 articles about 5-(tert-butyl-dimethyl-silanyloxy)-2-[2-(4-methoxyphenyl)-1-methyl-ethyl]-pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

: 1187188-77-7
5-(tert-butyl-dimethyl-silanyloxy)-2-[2-(4-methoxy-phenyl)-ethyl]-pyridine

: 74-88-4
methyl iodide

: 1187188-78-8
5-(tert-butyl-dimethyl-silanyloxy)-2-[2-(4-methoxyphenyl)-1-methyl-ethyl]-pyridine

Guidance literature:: 5-(tert-butyl-dimethyl-silanyloxy)-2-[2-(4-methoxy-phenyl)-ethyl]-pyridine; With lithium diisopropyl amide; In tetrahydrofuran; n-heptane; ethylbenzene; at -78 ℃; for 1h; Inert atmosphere;

methyl iodide; In tetrahydrofuran; ethylbenzene; pentane; at -78 - 20 ℃; for 3.5h; Inert atmosphere;
DOI:10.1016/j.ejmech.2009.03.013

Reference yield: 84.0%

: 1187188-78-8
5-(tert-butyl-dimethyl-silanyloxy)-2-[2-(4-methoxyphenyl)-1-methyl-ethyl]-pyridine

: 1187188-68-6
6-[2-(4-hydroxy-phenyl)-1-methyl-ethyl]-pyridin-3-ol

Guidance literature:: 5-(tert-butyl-dimethyl-silanyloxy)-2-[2-(4-methoxyphenyl)-1-methyl-ethyl]-pyridine; With water; hydrogen iodide; acetic acid; for 2.5h; Reflux;

With sodium hydroxide; sodium hydrogencarbonate; In water; at 20 ℃;
DOI:10.1016/j.ejmech.2009.03.013