PIPERIDINE, 1-(4-PIPERIDINYLCARBONYL)-, HYDROCHLORIDE

Base Information

• Chemical Name: PIPERIDINE, 1-(4-PIPERIDINYLCARBONYL)-, HYDROCHLORIDE
• CAS No.: 278598-12-2
• Molecular Formula: C₁₁H₂₀N₂O*ClH
• Molecular Weight: 232.754
• Hs Code.: 2933399090
• Mol file: 278598-12-2.mol

Synonyms:Piperidine,1-(4-piperidinylcarbonyl)-, monohydrochloride (9CI)

Chemical Property of PIPERIDINE, 1-(4-PIPERIDINYLCARBONYL)-, HYDROCHLORIDE

Chemical Property:

• PSA: 32.34000
• LogP: 2.06720

Purity/Quality:

97% ^*data from raw suppliers

1-Piperidinyl(4-piperidinyl)methanoneHydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of PIPERIDINE, 1-(4-PIPERIDINYLCARBONYL)-, HYDROCHLORIDE

There total 3 articles about PIPERIDINE, 1-(4-PIPERIDINYLCARBONYL)-, HYDROCHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

piperidin-1-yl(pyridin-4-yl)methanone (4968-87-0) → 1-(piperidin-4-ylcarbonyl)piperidine hydrochloride (278598-12-2)

Guidance literature:

With 1,1,2-trichloroethane; palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃; for 16h; under 760.051 Torr;

DOI:10.1016/j.tet.2009.08.011

Reference yield: 93.0%

→ 1-(piperidin-4-ylcarbonyl)piperidine hydrochloride (278598-12-2)

Guidance literature:

Reference yield:

4-(piperidine-1-carbonyl)-piperidine-1-carboxylic acid tert-butyl ester (757949-38-5) → 1-(piperidin-4-ylcarbonyl)piperidine hydrochloride (278598-12-2)

Guidance literature:

With hydrogenchloride; In ethyl acetate; at 20 ℃; Cooling with ice;

DOI:10.1021/jm9017916

upstream raw materials:

piperidin-1-yl(pyridin-4-yl)methanone

4-(piperidine-1-carbonyl)-piperidine-1-carboxylic acid tert-butyl ester

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