benzylsulfanyl-acetaldehyde dibenzyldithioacetal

Base Information

• Chemical Name: benzylsulfanyl-acetaldehyde dibenzyldithioacetal
• CAS No.: 247178-87-6
• Molecular Formula: C₂₃H₂₄S₃
• Molecular Weight: 396.642
• Mol file: 247178-87-6.mol

Synonyms:benzylsulfanyl-acetaldehyde dibenzyldithioacetal

Chemical Property of benzylsulfanyl-acetaldehyde dibenzyldithioacetal

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of benzylsulfanyl-acetaldehyde dibenzyldithioacetal

There total 2 articles about benzylsulfanyl-acetaldehyde dibenzyldithioacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phenylmethanethiol (100-53-8) → dibenzyl disulphide (150-60-7) + benzylsulfanyl-acetaldehyde dibenzyldithioacetal (247178-87-6)

Guidance literature:

With 1,4-dioxane; hydrogenchloride;

DOI:10.1002/hlca.19540370221

Reference yield:

1,2-bis-(benzylmercapto)ethylene (53959-54-9) + phenylmethanethiol (100-53-8) → benzylsulfanyl-acetaldehyde dibenzyldithioacetal (247178-87-6)

Guidance literature:

With sulfuric acid; acetic acid;

Reference yield:

benzylsulfanyl-acetaldehyde dibenzyldithioacetal (247178-87-6) → 1,2-bis-phenylmethanesulfonyl-ethane (101432-09-1)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether; permanganate; diluted sulfuric acid

2: zinc dust; glacial acetic acid

With diethyl ether; sulfuric acid; permanganate(VII) ion; acetic acid; zinc;

upstream raw materials:

1,2-bis-(benzylmercapto)ethylene

phenylmethanethiol

Downstream raw materials:

1-benzylsulfanyl-1,2-bis-phenylmethanesulfonyl-ethane

1,2-bis-phenylmethanesulfonyl-ethane