N-<4-phenyl>-2-<(4-carboxy-2,6-dinitrophenyl)amino>propanamide

Base Information

Chemical Name:N-<4-phenyl>-2-<(4-carboxy-2,6-dinitrophenyl)amino>propanamide
CAS No.:220903-73-1
Molecular Formula:C₂₀H₂₁Cl₂N₅O₇
Molecular Weight:514.322
Hs Code.:

N-<4-<bis(2-chloroethyl)amino>phenyl>-2-<(4-carboxy-2,6-dinitrophenyl)amino>propanamide

Synonyms:N-<4-phenyl>-2-<(4-carboxy-2,6-dinitrophenyl)amino>propanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<4-phenyl>-2-<(4-carboxy-2,6-dinitrophenyl)amino>propanamide

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Technology Process of N-<4-phenyl>-2-<(4-carboxy-2,6-dinitrophenyl)amino>propanamide

There total 3 articles about N-<4-phenyl>-2-<(4-carboxy-2,6-dinitrophenyl)amino>propanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 220903-72-0
2-amino-N-<4-phenyl>propanamide

: 118-97-8
4-chloro-3,5-dinitrobenzoic acid

: 220903-73-1
N-<4-phenyl>-2-<(4-carboxy-2,6-dinitrophenyl)amino>propanamide

Guidance literature:: With diisopropylamine; In tetrahydrofuran; at 20 ℃; for 12h;
DOI:10.1021/jm960783s

Reference yield:

: 945-68-6
N,N-bis(2-chloroethyl)benzene-1,4-diamine hydrochloride

: 220903-73-1
N-<4-phenyl>-2-<(4-carboxy-2,6-dinitrophenyl)amino>propanamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) ethyl cyanophosphonate, 2.) diisopropylethylamine / 1.) DMF, 0 deg C, 2.) DMF, 20 deg C, 1.5 h

2: 93 percent / TFA / 2 h / 20 °C

3: 71 percent / diisopropylamine / tetrahydrofuran / 12 h / 20 °C

With diethyl cyanophosphonate; diisopropylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran;
DOI:10.1021/jm960783s

Reference yield:

: 220903-71-9
N-<4-phenyl>-2-(tert-butyloxycarbonylamino)propanamide

: 220903-73-1
N-<4-phenyl>-2-<(4-carboxy-2,6-dinitrophenyl)amino>propanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / TFA / 2 h / 20 °C

2: 71 percent / diisopropylamine / tetrahydrofuran / 12 h / 20 °C

With diisopropylamine; trifluoroacetic acid; In tetrahydrofuran;
DOI:10.1021/jm960783s