2-{1-(tert-butyldimethylsilanyloxymethyl)-2-[4-(tert-butyldimethylsilanyloxy)phenyl]ethylamino}[1,4]naphthoquinone

Base Information

Chemical Name:2-{1-(tert-butyldimethylsilanyloxymethyl)-2-[4-(tert-butyldimethylsilanyloxy)phenyl]ethylamino}[1,4]naphthoquinone
CAS No.:613223-57-7
Molecular Formula:C₃₁H₄₅NO₄Si₂
Molecular Weight:551.874
Hs Code.:

Synonyms:2-{1-(tert-butyldimethylsilanyloxymethyl)-2-[4-(tert-butyldimethylsilanyloxy)phenyl]ethylamino}[1,4]naphthoquinone

Suppliers and Price of 2-{1-(tert-butyldimethylsilanyloxymethyl)-2-[4-(tert-butyldimethylsilanyloxy)phenyl]ethylamino}[1,4]naphthoquinone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-{1-(tert-butyldimethylsilanyloxymethyl)-2-[4-(tert-butyldimethylsilanyloxy)phenyl]ethylamino}[1,4]naphthoquinone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-{1-(tert-butyldimethylsilanyloxymethyl)-2-[4-(tert-butyldimethylsilanyloxy)phenyl]ethylamino}[1,4]naphthoquinone

There total 4 articles about 2-{1-(tert-butyldimethylsilanyloxymethyl)-2-[4-(tert-butyldimethylsilanyloxy)phenyl]ethylamino}[1,4]naphthoquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 613223-66-8
2-[1-hydroxymethyl-2-(4-hydroxyphenyl)ethylamino][1,4]naphthoquinone

: 613223-57-7
2-{1-(tert-butyldimethylsilanyloxymethyl)-2-[4-(tert-butyldimethylsilanyloxy)phenyl]ethylamino}[1,4]naphthoquinone

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1021/ja0365330

Reference yield:

: 1080-06-4,3410-66-0,18869-47-1
tyrosine methyl ester

: 613223-57-7
2-{1-(tert-butyldimethylsilanyloxymethyl)-2-[4-(tert-butyldimethylsilanyloxy)phenyl]ethylamino}[1,4]naphthoquinone

Guidance literature:: Multi-step reaction with 3 steps

1: 57 percent / methanol / 12 h / 20 °C

2: 100 percent / LiBH₄ / tetrahydrofuran / 2 h / 20 °C

3: 100 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / CH₂Cl₂ / 1 h / 20 °C

With lithium borohydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ja0365330

Reference yield:

: 130-15-4
[1,4]naphthoquinone

: 613223-57-7
2-{1-(tert-butyldimethylsilanyloxymethyl)-2-[4-(tert-butyldimethylsilanyloxy)phenyl]ethylamino}[1,4]naphthoquinone

Guidance literature:: Multi-step reaction with 3 steps

1: 57 percent / methanol / 12 h / 20 °C

2: 100 percent / LiBH₄ / tetrahydrofuran / 2 h / 20 °C

3: 100 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / CH₂Cl₂ / 1 h / 20 °C

With lithium borohydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ja0365330