cyclohexyl 4-hydroxy-4-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cis-cyclohexyl carbonate

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Chemical Name:cyclohexyl 4-hydroxy-4-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cis-cyclohexyl carbonate
CAS No.:1224949-12-5
Molecular Formula:C₃₀H₃₆N₂O₅
Molecular Weight:504.626
Hs Code.:

Synonyms:cyclohexyl 4-hydroxy-4-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cis-cyclohexyl carbonate

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Chemical Property of cyclohexyl 4-hydroxy-4-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cis-cyclohexyl carbonate

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Technology Process of cyclohexyl 4-hydroxy-4-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cis-cyclohexyl carbonate

There total 8 articles about cyclohexyl 4-hydroxy-4-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cis-cyclohexyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 1224948-06-4
1-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)cyclohexane-cis-1,4-diol

: 95789-69-8,102672-57-1
cyclohexyl (1-iodoethyl)carbonate

: 1224949-12-5
cyclohexyl 4-hydroxy-4-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cis-cyclohexyl carbonate

Guidance literature:: 1-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)cyclohexane-cis-1,4-diol; With sodium hydride; In tetrahydrofuran; for 0.166667h; Cooling with ice;

cyclohexyl (1-iodoethyl)carbonate; In tetrahydrofuran; at 20 ℃; for 12h;

Reference yield:

: 4746-97-8
cyclohexanedione monoethylene ketal

: 1224949-12-5
cyclohexyl 4-hydroxy-4-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cis-cyclohexyl carbonate

Guidance literature:: Multi-step reaction with 8 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -76 °C

1.2: 2 h / -74 °C

2.1: potassium carbonate; methanol / 2 h / 20 °C

3.1: n-butyllithium / hexane; tetrahydrofuran / 0.92 h / -72 °C

3.2: 0.58 h / -72 °C

4.1: manganese(IV) oxide / dichloromethane / 15 h / 20 °C

5.1: triethylamine / ethanol / 0.5 h / 20 °C

5.2: 15 h / 20 °C

6.1: hydrogenchloride; water / tetrahydrofuran / 15 h / 20 °C

6.2: 0 °C

7.1: sodium tetrahydroborate; methanol / 2 h / 20 °C

8.1: sodium hydride / tetrahydrofuran / 0.17 h / Cooling with ice

8.2: 12 h / 20 °C

With hydrogenchloride; methanol; manganese(IV) oxide; sodium tetrahydroborate; n-butyllithium; water; sodium hydride; potassium carbonate; triethylamine; In tetrahydrofuran; ethanol; hexane; dichloromethane;

Reference yield:

: 70097-74-4
8-ethynyl-1,4-dioxaspiro[4.5]decan-8-ol

: 1224949-12-5
cyclohexyl 4-hydroxy-4-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cis-cyclohexyl carbonate

Guidance literature:: Multi-step reaction with 6 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 0.92 h / -72 °C

1.2: 0.58 h / -72 °C

2.1: manganese(IV) oxide / dichloromethane / 15 h / 20 °C

3.1: triethylamine / ethanol / 0.5 h / 20 °C

3.2: 15 h / 20 °C

4.1: hydrogenchloride; water / tetrahydrofuran / 15 h / 20 °C

4.2: 0 °C

5.1: sodium tetrahydroborate; methanol / 2 h / 20 °C

6.1: sodium hydride / tetrahydrofuran / 0.17 h / Cooling with ice

6.2: 12 h / 20 °C

With hydrogenchloride; methanol; manganese(IV) oxide; sodium tetrahydroborate; n-butyllithium; water; sodium hydride; triethylamine; In tetrahydrofuran; ethanol; hexane; dichloromethane;