(2S,3R)-3-hydroxy-2-(4-nitrobenzenesulfonyloxy)-3-phenylpropionic acid methyl ester

Base Information

Chemical Name:(2S,3R)-3-hydroxy-2-(4-nitrobenzenesulfonyloxy)-3-phenylpropionic acid methyl ester
CAS No.:132377-67-4
Molecular Formula:C₁₆H₁₅NO₈S
Molecular Weight:381.363
Hs Code.:

Synonyms:(2S,3R)-3-hydroxy-2-(4-nitrobenzenesulfonyloxy)-3-phenylpropionic acid methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3R)-3-hydroxy-2-(4-nitrobenzenesulfonyloxy)-3-phenylpropionic acid methyl ester

Chemical Property:

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Technology Process of (2S,3R)-3-hydroxy-2-(4-nitrobenzenesulfonyloxy)-3-phenylpropionic acid methyl ester

There total 2 articles about (2S,3R)-3-hydroxy-2-(4-nitrobenzenesulfonyloxy)-3-phenylpropionic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 124649-67-8
methyl (2S,3R)-3-phenyl-2,3-dihydroxypropanoate

: 98-74-8
4-Nitrobenzenesulfonyl chloride

: 132377-67-4
(2S,3R)-3-hydroxy-2-(4-nitrobenzenesulfonyloxy)-3-phenylpropionic acid methyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1002/chem.201301120

Reference yield:

: 103-26-4,1754-62-7
Methyl cinnamate

: 132377-67-4
(2S,3R)-3-hydroxy-2-(4-nitrobenzenesulfonyloxy)-3-phenylpropionic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: AD-mix-β; methanesulfonamide; water / tert-butyl alcohol / 18 h / 20 °C

2: triethylamine / dichloromethane / 1 h / 0 °C

With methanesulfonamide; AD-mix-β; water; triethylamine; In dichloromethane; tert-butyl alcohol;
DOI:10.1002/chem.201301120