allyl-[3-(4-benzyl-2-oxo-oxazolidin-3-yl)-3-oxo-propyl]-carbamic acid tert-butyl ester

Base Information

• Chemical Name: allyl-[3-(4-benzyl-2-oxo-oxazolidin-3-yl)-3-oxo-propyl]-carbamic acid tert-butyl ester
• CAS No.: 851593-73-2
• Molecular Formula: C₂₁H₂₈N₂O₅
• Molecular Weight: 388.464

Synonyms:allyl-[3-(4-benzyl-2-oxo-oxazolidin-3-yl)-3-oxo-propyl]-carbamic acid tert-butyl ester

Chemical Property of allyl-[3-(4-benzyl-2-oxo-oxazolidin-3-yl)-3-oxo-propyl]-carbamic acid tert-butyl ester

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Technology Process of allyl-[3-(4-benzyl-2-oxo-oxazolidin-3-yl)-3-oxo-propyl]-carbamic acid tert-butyl ester

There total 3 articles about allyl-[3-(4-benzyl-2-oxo-oxazolidin-3-yl)-3-oxo-propyl]-carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-(allyl-tert-butoxycarbonyl-amino)-propionic acid (355390-94-2) → allyl-[3-(4-benzyl-2-oxo-oxazolidin-3-yl)-3-oxo-propyl]-carbamic acid tert-butyl ester (851593-73-2)

Guidance literature:

Multi-step reaction with 2 steps

1: Et₃N / tetrahydrofuran

2: n-BuLi

With n-butyllithium; triethylamine; In tetrahydrofuran;

DOI:10.1055/s-2005-863719

Reference yield:

ethyl 3-(prop-2-en-1-ylamino)propanoate (44981-87-5) → allyl-[3-(4-benzyl-2-oxo-oxazolidin-3-yl)-3-oxo-propyl]-carbamic acid tert-butyl ester (851593-73-2)

Guidance literature:

Multi-step reaction with 4 steps

1: CH₂Cl₂ / 20 °C

2: aq. NaOH / tetrahydrofuran; ethanol / 20 °C

3: Et₃N / tetrahydrofuran

4: n-BuLi

With sodium hydroxide; n-butyllithium; triethylamine; In tetrahydrofuran; ethanol; dichloromethane;

DOI:10.1055/s-2005-863719

Reference yield:

ethyl 3-(allyl(tert-butoxycarbonyl)amino)propanoate (355390-78-2) → allyl-[3-(4-benzyl-2-oxo-oxazolidin-3-yl)-3-oxo-propyl]-carbamic acid tert-butyl ester (851593-73-2)

Guidance literature:

Multi-step reaction with 3 steps

1: aq. NaOH / tetrahydrofuran; ethanol / 20 °C

2: Et₃N / tetrahydrofuran

3: n-BuLi

With sodium hydroxide; n-butyllithium; triethylamine; In tetrahydrofuran; ethanol;

DOI:10.1055/s-2005-863719

upstream raw materials:

3-(allyl-tert-butoxycarbonyl-amino)-propionic acid

ethyl 3-(prop-2-en-1-ylamino)propanoate

ethyl 3-(allyl(tert-butoxycarbonyl)amino)propanoate

Downstream raw materials:

Allyl-[(R)-2-((R)-4-benzyl-2-oxo-oxazolidine-3-carbonyl)-pent-4-enyl]-carbamic acid tert-butyl ester

(R)-3-((R)-4-Benzyl-2-oxo-oxazolidine-3-carbonyl)-2,3,4,7-tetrahydro-azepine-1-carboxylic acid tert-butyl ester

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