C₅₉H₆₃NO₁₇

Base Information

Chemical Name:C₅₉H₆₃NO₁₇
CAS No.:266676-48-6
Molecular Formula:C₅₉H₆₃NO₁₇
Molecular Weight:1058.15
Hs Code.:

C<sub>59</sub>H<sub>63</sub>NO<sub>17</sub>

Synonyms:C₅₉H₆₃NO₁₇

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Chemical Property of C₅₉H₆₃NO₁₇

Chemical Property:

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Technology Process of C₅₉H₆₃NO₁₇

There total 17 articles about C₅₉H₆₃NO₁₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 266676-47-5
C₆₆H₆₉NO₁₇

: 266676-48-6
C₅₉H₆₃NO₁₇

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; at 20 ℃;
DOI:10.1016/S0960-894X(00)00031-7

Reference yield:

: 11034-45-0
1β,2α,9α,10β-tetrahydroxy-5α-cinnamoyloxytaxa-4(20),11-dien-13-one

: 266676-48-6
C₅₉H₆₃NO₁₇

Guidance literature:: Multi-step reaction with 16 steps

1: 73 percent / CuSO₄

2: 92 percent / pyridine / CH₂Cl₂ / 0 °C

3: 65 percent / aq. H₂NOH*HCl; NaOAc / ethanol / Heating

4: 86 percent / aq. OsO₄; NMO / tetrahydrofuran / 20 °C

5: 95 percent / imidazole / dimethylformamide / 20 °C

6: 81 percent / pyridine

7: TBAF / tetrahydrofuran

8: Bu₄N⁺AcO^- / butan-2-one / Heating

9: 71 percent / aq. AcOH / tetrahydrofuran / 40 °C

10: 76 percent / DMAP / 0 - 20 °C

11: 84 percent / tetrahydrofuran / -78 °C

12: 69 percent / DMAP / dimethylformamide / 48 h / 85 °C

13: 90 percent / DCC; DMAP / toluene

14: 83 percent / NaBH₄ / methanol / 20 °C

15: 86 percent / DCC; DMAP / toluene

16: 73 percent / H₂ / 10 percent Pd/C / ethyl acetate / 20 °C

With pyridine; 1H-imidazole; dmap; sodium tetrahydroborate; osmium(VIII) oxide; N-methyl-2-indolinone; hydroxylamine hydrochloride; tetrabutyl ammonium fluoride; hydrogen; sodium acetate; tetrabutylammonium acetate; copper(II) sulfate; acetic acid; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene; butanone; 1: ketalization / 2: cyclocondensation / 3: Hydrolysis / 4: dihydroxylation / 5: silylation / 6: mesylation / 7: desilylation / 8: Cyclization / 9: deketalization / 10: Acetylation / 11: Addition / 12: Addition / 13: Esterification / 14: Reduction / 15: Esterification / 16: Hydrogenolysis;
DOI:10.1016/S0960-894X(00)00031-7

Reference yield:

: 13452-36-3
2,9,10-triacetyl-5-O-cinnamoyltaxicin-I

: 266676-48-6
C₅₉H₆₃NO₁₇

Guidance literature:: Multi-step reaction with 17 steps

1: 86 percent / NaOCH₃ / methanol; CH₂Cl₂ / 0 °C

2: 73 percent / CuSO₄

3: 92 percent / pyridine / CH₂Cl₂ / 0 °C

4: 65 percent / aq. H₂NOH*HCl; NaOAc / ethanol / Heating

5: 86 percent / aq. OsO₄; NMO / tetrahydrofuran / 20 °C

6: 95 percent / imidazole / dimethylformamide / 20 °C

7: 81 percent / pyridine

8: TBAF / tetrahydrofuran

9: Bu₄N⁺AcO^- / butan-2-one / Heating

10: 71 percent / aq. AcOH / tetrahydrofuran / 40 °C

11: 76 percent / DMAP / 0 - 20 °C

12: 84 percent / tetrahydrofuran / -78 °C

13: 69 percent / DMAP / dimethylformamide / 48 h / 85 °C

14: 90 percent / DCC; DMAP / toluene

15: 83 percent / NaBH₄ / methanol / 20 °C

16: 86 percent / DCC; DMAP / toluene

17: 73 percent / H₂ / 10 percent Pd/C / ethyl acetate / 20 °C

With pyridine; 1H-imidazole; dmap; sodium tetrahydroborate; osmium(VIII) oxide; N-methyl-2-indolinone; hydroxylamine hydrochloride; tetrabutyl ammonium fluoride; hydrogen; sodium methylate; sodium acetate; tetrabutylammonium acetate; copper(II) sulfate; acetic acid; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene; butanone; 1: Deacetylation / 2: ketalization / 3: cyclocondensation / 4: Hydrolysis / 5: dihydroxylation / 6: silylation / 7: mesylation / 8: desilylation / 9: Cyclization / 10: deketalization / 11: Acetylation / 12: Addition / 13: Addition / 14: Esterification / 15: Reduction / 16: Esterification / 17: Hydrogenolysis;
DOI:10.1016/S0960-894X(00)00031-7