Technology Process of 3,3,3-trifluoro-2-methyl-1,1-diphenylpropene
There total 4 articles about 3,3,3-trifluoro-2-methyl-1,1-diphenylpropene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tris(2,2-bipyridine)ruthenium(II) hexafluorophosphate;
In
dimethyl sulfoxide;
at 20 ℃;
for 2h;
Schlenk technique;
Inert atmosphere;
Irradiation;
DOI:10.3762/bjoc.10.108
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hexamethyldisilazane / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere
1.2: 20 °C / Inert atmosphere
2.1: tris(2,2-bipyridine)ruthenium(II) hexafluorophosphate / dimethyl sulfoxide / 2 h / 20 °C / Schlenk technique; Inert atmosphere; Irradiation
With
tris(2,2-bipyridine)ruthenium(II) hexafluorophosphate; sodium hexamethyldisilazane;
In
tetrahydrofuran; dimethyl sulfoxide;
1.1: |Wittig Olefination / 1.2: |Wittig Olefination;
DOI:10.3762/bjoc.10.108
- Guidance literature:
-
With
palladium catalyst;
In
1,4-dioxane;
Reflux;
Inert atmosphere;
Alkaline conditions;
DOI:10.1246/cl.2010.867
