Technology Process of C21H19NO6
There total 7 articles about C21H19NO6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
lithium tri-t-butoxyaluminum hydride;
In
tetrahydrofuran;
at -30 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: ethylene glycol; sodium hydrogencarbonate; potassium permanganate / water; acetone / 2 h / -15 - -10 °C / Large scale
2.1: triethylamine; thionyl chloride / dichloromethane / 1.5 h / -5 - 25 °C / Large scale
3.1: water; sodium hypochlorite / dichloromethane; acetonitrile / 41 h / 5 - 25 °C / Large scale
4.1: N,N-dimethyl-formamide; water / 5 h / 50 °C / Large scale
4.2: 30 °C / Large scale
5.1: hydrogenchloride / ethanol / 15 h / 20 - 30 °C
6.1: triethylamine; dmap / acetonitrile / 2.5 h / 0 - 25 °C
7.1: lithium tri-t-butoxyaluminum hydride / tetrahydrofuran / 2 h / -30 °C
With
hydrogenchloride; dmap; sodium hypochlorite; potassium permanganate; thionyl chloride; water; sodium hydrogencarbonate; ethylene glycol; lithium tri-t-butoxyaluminum hydride; triethylamine;
In
tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: water; sodium hypochlorite / dichloromethane; acetonitrile / 41 h / 5 - 25 °C / Large scale
2.1: N,N-dimethyl-formamide; water / 5 h / 50 °C / Large scale
2.2: 30 °C / Large scale
3.1: hydrogenchloride / ethanol / 15 h / 20 - 30 °C
4.1: triethylamine; dmap / acetonitrile / 2.5 h / 0 - 25 °C
5.1: lithium tri-t-butoxyaluminum hydride / tetrahydrofuran / 2 h / -30 °C
With
hydrogenchloride; dmap; sodium hypochlorite; water; lithium tri-t-butoxyaluminum hydride; triethylamine;
In
tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;