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C21H19NO6

Base Information Edit
C<sub>21</sub>H<sub>19</sub>NO<sub>6</sub>

Synonyms:C21H19NO6

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The product has achieved commercial mass production*data from LookChem market partment
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Chemical Property of C21H19NO6 Edit
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Technology Process of C21H19NO6

There total 7 articles about C21H19NO6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With lithium tri-t-butoxyaluminum hydride; In tetrahydrofuran; at -30 ℃; for 2h;
Guidance literature:
Multi-step reaction with 7 steps
1.1: ethylene glycol; sodium hydrogencarbonate; potassium permanganate / water; acetone / 2 h / -15 - -10 °C / Large scale
2.1: triethylamine; thionyl chloride / dichloromethane / 1.5 h / -5 - 25 °C / Large scale
3.1: water; sodium hypochlorite / dichloromethane; acetonitrile / 41 h / 5 - 25 °C / Large scale
4.1: N,N-dimethyl-formamide; water / 5 h / 50 °C / Large scale
4.2: 30 °C / Large scale
5.1: hydrogenchloride / ethanol / 15 h / 20 - 30 °C
6.1: triethylamine; dmap / acetonitrile / 2.5 h / 0 - 25 °C
7.1: lithium tri-t-butoxyaluminum hydride / tetrahydrofuran / 2 h / -30 °C
With hydrogenchloride; dmap; sodium hypochlorite; potassium permanganate; thionyl chloride; water; sodium hydrogencarbonate; ethylene glycol; lithium tri-t-butoxyaluminum hydride; triethylamine; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile;
Guidance literature:
Multi-step reaction with 5 steps
1.1: water; sodium hypochlorite / dichloromethane; acetonitrile / 41 h / 5 - 25 °C / Large scale
2.1: N,N-dimethyl-formamide; water / 5 h / 50 °C / Large scale
2.2: 30 °C / Large scale
3.1: hydrogenchloride / ethanol / 15 h / 20 - 30 °C
4.1: triethylamine; dmap / acetonitrile / 2.5 h / 0 - 25 °C
5.1: lithium tri-t-butoxyaluminum hydride / tetrahydrofuran / 2 h / -30 °C
With hydrogenchloride; dmap; sodium hypochlorite; water; lithium tri-t-butoxyaluminum hydride; triethylamine; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
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