Benzoic acid, 4-amino-3-hydroxy-, 2-propenyl ester (9CI)

Base Information

Chemical Name:Benzoic acid, 4-amino-3-hydroxy-, 2-propenyl ester (9CI)
CAS No.:273939-62-1
Molecular Formula:C10H11 N O3
Molecular Weight:193.19924
Hs Code.:
Mol file:273939-62-1.mol

Synonyms:Benzoicacid, 4-amino-3-hydroxy-, 2-propenyl ester (9CI)

Suppliers and Price of Benzoic acid, 4-amino-3-hydroxy-, 2-propenyl ester (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Benzoic acid, 4-amino-3-hydroxy-, 2-propenyl ester (9CI)

Chemical Property:

Boiling Point:388.7±32.0 °C(Predicted)
PKA:8.92±0.10(Predicted)
PSA：72.55000
Density:1.237±0.06 g/cm3(Predicted)
LogP:1.89840

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzoic acid, 4-amino-3-hydroxy-, 2-propenyl ester (9CI)

There total 1 articles about Benzoic acid, 4-amino-3-hydroxy-, 2-propenyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2374-03-0
4-aminosalicylic acid

: 106-95-6
allyl bromide

: 273939-62-1
allyl 4-amino-3-hydroxybenzoate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1021/acsmedchemlett.5b00218

Reference yield: 65.0%

: 4530-20-5
BOC-glycine

: 273939-62-1
allyl 4-amino-3-hydroxybenzoate

: 1258644-44-8
C₁₇H₂₂N₂O₆

Guidance literature:: With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1021/co100056c

Reference yield:

: 273939-62-1
allyl 4-amino-3-hydroxybenzoate

: 1258644-51-7
C₁₉H₂₀N₂O₄

Guidance literature:: Multi-step reaction with 3 steps

1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 12 h / 20 °C

2: sodium hydride / N,N-dimethyl-formamide / 3 h / 20 °C

3: trifluoroacetic acid / dichloromethane / 4 h / 20 °C

With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; sodium hydride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/co100056c