1-[2-(6-chloropyridin-3-ylmethoxy)-benzoyl]-3-(2-nitrophenyl)thiourea

Base Information

Chemical Name:1-[2-(6-chloropyridin-3-ylmethoxy)-benzoyl]-3-(2-nitrophenyl)thiourea
CAS No.:1607026-77-6
Molecular Formula:C₂₀H₁₅ClN₄O₄S
Molecular Weight:442.882
Hs Code.:

Synonyms:1-[2-(6-chloropyridin-3-ylmethoxy)-benzoyl]-3-(2-nitrophenyl)thiourea

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Chemical Property of 1-[2-(6-chloropyridin-3-ylmethoxy)-benzoyl]-3-(2-nitrophenyl)thiourea

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Technology Process of 1-[2-(6-chloropyridin-3-ylmethoxy)-benzoyl]-3-(2-nitrophenyl)thiourea

There total 5 articles about 1-[2-(6-chloropyridin-3-ylmethoxy)-benzoyl]-3-(2-nitrophenyl)thiourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: C₁₄H₉ClN₂O₂S

: 88-74-4
2-nitro-aniline

: 1607026-77-6
1-[2-(6-chloropyridin-3-ylmethoxy)-benzoyl]-3-(2-nitrophenyl)thiourea

Guidance literature:: In acetonitrile; at 60 - 70 ℃; for 3h;
DOI:10.2174/15701808113109990045

Reference yield:

: 69-72-7,25496-36-0,8052-31-1
salicylic acid

: 1607026-77-6
1-[2-(6-chloropyridin-3-ylmethoxy)-benzoyl]-3-(2-nitrophenyl)thiourea

Guidance literature:: Multi-step reaction with 5 steps

1: sulfuric acid

2: potassium carbonate / acetonitrile

3: sodium hydroxide; water / methanol

4: acetonitrile

5: acetonitrile / 3 h / 60 - 70 °C

With sulfuric acid; water; potassium carbonate; sodium hydroxide; In methanol; acetonitrile;
DOI:10.2174/15701808113109990045

Reference yield:

: 119-36-8,8024-54-2
methyl salicylate

: 1607026-77-6
1-[2-(6-chloropyridin-3-ylmethoxy)-benzoyl]-3-(2-nitrophenyl)thiourea

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / acetonitrile

2: sodium hydroxide; water / methanol

3: acetonitrile

4: acetonitrile / 3 h / 60 - 70 °C

With water; potassium carbonate; sodium hydroxide; In methanol; acetonitrile;
DOI:10.2174/15701808113109990045