C₁₉H₁₉NO₄S

Base Information

Chemical Name:C₁₉H₁₉NO₄S
CAS No.:1394159-31-9
Molecular Formula:C₁₉H₁₉NO₄S
Molecular Weight:357.43
Hs Code.:

C<sub>19</sub>H<sub>19</sub>NO<sub>4</sub>S

Synonyms:C₁₉H₁₉NO₄S

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Chemical Property of C₁₉H₁₉NO₄S

Chemical Property:

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Technology Process of C₁₉H₁₉NO₄S

There total 3 articles about C₁₉H₁₉NO₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1394159-21-7
C₂₃H₂₇NO₄S

: 1394159-31-9
C₁₉H₁₉NO₄S

Guidance literature:: With formic acid; at 20 ℃;
DOI:10.1016/j.tetlet.2012.06.075

Reference yield:

: 100-58-3
phenylmagnesium bromide

: 1394159-31-9
C₁₉H₁₉NO₄S

Guidance literature:: Multi-step reaction with 4 steps

1.1: copper(l) iodide / diethyl ether / -78 °C / Inert atmosphere

1.2: -60 - 20 °C

2.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 20 °C

3.1: tetrabutylammomium bromide; palladium diacetate; sodium carbonate; triphenylphosphine / 1,4-dioxane / 14 h / 100 °C / Inert atmosphere

4.1: formic acid / 20 °C

With copper(l) iodide; formic acid; di-isopropyl azodicarboxylate; tetrabutylammomium bromide; palladium diacetate; sodium carbonate; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; diethyl ether; 2.1: Mitsunobu reaction / 3.1: Heck-aza-Michael reaction;
DOI:10.1016/j.tetlet.2012.06.075

Reference yield:

: 1287655-99-5
C₁₆H₁₆INO₂S

: 1394159-31-9
C₁₉H₁₉NO₄S

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutylammomium bromide; palladium diacetate; sodium carbonate; triphenylphosphine / 1,4-dioxane / 14 h / 100 °C / Inert atmosphere

2: formic acid / 20 °C

With formic acid; tetrabutylammomium bromide; palladium diacetate; sodium carbonate; triphenylphosphine; In 1,4-dioxane; 1: Heck-aza-Michael reaction;
DOI:10.1016/j.tetlet.2012.06.075