4,5,6,7-tetrahydro-1,3a,3b,8-tetraaza-cyclopenta[a]indene-2-carbaldehyde

Base Information

Chemical Name:4,5,6,7-tetrahydro-1,3a,3b,8-tetraaza-cyclopenta[a]indene-2-carbaldehyde
CAS No.:623906-41-2
Molecular Formula:C₉H₁₀N₄O
Molecular Weight:190.205
Hs Code.:

Synonyms:4,5,6,7-tetrahydro-1,3a,3b,8-tetraaza-cyclopenta[a]indene-2-carbaldehyde

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Chemical Property of 4,5,6,7-tetrahydro-1,3a,3b,8-tetraaza-cyclopenta[a]indene-2-carbaldehyde

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Technology Process of 4,5,6,7-tetrahydro-1,3a,3b,8-tetraaza-cyclopenta[a]indene-2-carbaldehyde

There total 2 articles about 4,5,6,7-tetrahydro-1,3a,3b,8-tetraaza-cyclopenta[a]indene-2-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 623906-40-1
4,5,6,7-tetrahydro-1,3a,3b,8-tetraazacyclopenta[a]indene-2-carboxylic acid ethyl ester

: 623906-41-2
4,5,6,7-tetrahydro-1,3a,3b,8-tetraaza-cyclopenta[a]indene-2-carbaldehyde

Guidance literature:: 4,5,6,7-tetrahydro-1,3a,3b,8-tetraazacyclopenta[a]indene-2-carboxylic acid ethyl ester; With diisobutylaluminium hydride; In tetrahydrofuran; toluene; at -78 - 0 ℃; for 1.5h;

With water; ammonium chloride; In tetrahydrofuran; ethyl acetate; toluene; for 0.0833333h; Sonification;

Reference yield: 58.0%

: 623906-40-1
4,5,6,7-tetrahydro-1,3a,3b,8-tetraazacyclopenta[a]indene-2-carboxylic acid ethyl ester

: 1191-15-7
diisobutylaluminium hydride

: 623906-41-2
4,5,6,7-tetrahydro-1,3a,3b,8-tetraaza-cyclopenta[a]indene-2-carbaldehyde

Guidance literature:: With ammonium chloride; In tetrahydrofuran; ethanol; toluene;

Reference yield: 13.0%

: 623906-41-2
4,5,6,7-tetrahydro-1,3a,3b,8-tetraaza-cyclopenta[a]indene-2-carbaldehyde

: 108-24-7
acetic anhydride

: 623564-16-9
(5R,6S)-6-bromo-7-oxo-4-thia-1-aza-bicyclo[3.2.0]hept-2-ene-2-carboxylic acid 4-nitrobenzyl ester

: 623906-42-3
(5R,6RS)-6-{(RS)-acetyloxy-[4,5,6,7-tetrahydro-1,3a,3b,8-tetraaza-cyclopenta[a]inden-2-yl]methyl}-6-bromo-7-oxo-4-thia-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylic acid 4-nitrobenzyl ester

Guidance literature:: 4,5,6,7-tetrahydro-1,3a,3b,8-tetraaza-cyclopenta[a]indene-2-carbaldehyde; (5R,6S)-6-bromo-7-oxo-4-thia-1-aza-bicyclo[3.2.0]hept-2-ene-2-carboxylic acid 4-nitrobenzyl ester; With triethylamine; magnesium bromide; In tetrahydrofuran; acetonitrile; at -20 - 20 ℃; for 1.2h; Darkness;

acetic anhydride; In tetrahydrofuran; acetonitrile; at 0 ℃; for 16h;