C₄₃H₄₅N₃O₈S

Base Information

• Chemical Name: C₄₃H₄₅N₃O₈S
• CAS No.: 1350319-85-5
• Molecular Formula: C₄₃H₄₅N₃O₈S
• Molecular Weight: 763.912
• Mol file: 1350319-85-5.mol

Synonyms:C₄₃H₄₅N₃O₈S

Chemical Property of C₄₃H₄₅N₃O₈S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₃H₄₅N₃O₈S

There total 5 articles about C₄₃H₄₅N₃O₈S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

C47H53N3O8S (1350319-84-4) → C43H45N3O8S (1350319-85-5)

Guidance literature:

With toluene-4-sulfonic acid; In toluene; at 80 ℃; for 6h;

Reference yield:

4-bromo-aniline (106-40-1) → C43H45N3O8S (1350319-85-5)

Guidance literature:

Multi-step reaction with 5 steps

1: 1,10-Phenanthroline; copper(l) chloride; potassium hydroxide / toluene / 24 h / 100 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 40 h / Reflux

3: acetonitrile / 20 h / 20 °C

4: potassium carbonate / 1,4-dioxane / 4 h / 80 °C

5: toluene-4-sulfonic acid / toluene / 6 h / 80 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1,10-Phenanthroline; potassium carbonate; toluene-4-sulfonic acid; copper(l) chloride; potassium hydroxide; In 1,4-dioxane; toluene; acetonitrile;

Reference yield:

N,N-bis(4-hexyloxyphenyl)-4-bromophenylamine (1092363-75-1) → C43H45N3O8S (1350319-85-5)

Guidance literature:

Multi-step reaction with 4 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 40 h / Reflux

2: acetonitrile / 20 h / 20 °C

3: potassium carbonate / 1,4-dioxane / 4 h / 80 °C

4: toluene-4-sulfonic acid / toluene / 6 h / 80 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; toluene-4-sulfonic acid; In 1,4-dioxane; toluene; acetonitrile;

upstream raw materials:

4-bromo-aniline

N,N-bis(4-hexyloxyphenyl)-4-bromophenylamine

2-[4-[N,N-bis-(4-hexyloxyphenyl)amino]phenyl]-3,4-(ethylenedioxy)thiophene

C₄₁H₄₃N₃O₆S

Refernces