1-[4-(4-{4-[(6-amino-9H-purin-9-yl)methyl]phenyl}butyl)benzyl]-4-pyrrolidinopyridinium bromide

Base Information

Chemical Name:1-[4-(4-{4-[(6-amino-9H-purin-9-yl)methyl]phenyl}butyl)benzyl]-4-pyrrolidinopyridinium bromide
CAS No.:1365671-67-5
Molecular Formula:Br*C₃₂H₃₆N₇
Molecular Weight:598.589
Hs Code.:

Synonyms:1-[4-(4-{4-[(6-amino-9H-purin-9-yl)methyl]phenyl}butyl)benzyl]-4-pyrrolidinopyridinium bromide

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Chemical Property of 1-[4-(4-{4-[(6-amino-9H-purin-9-yl)methyl]phenyl}butyl)benzyl]-4-pyrrolidinopyridinium bromide

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Technology Process of 1-[4-(4-{4-[(6-amino-9H-purin-9-yl)methyl]phenyl}butyl)benzyl]-4-pyrrolidinopyridinium bromide

There total 4 articles about 1-[4-(4-{4-[(6-amino-9H-purin-9-yl)methyl]phenyl}butyl)benzyl]-4-pyrrolidinopyridinium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 1365672-08-7
1-(4-{4-[4-(bromomethyl)phenyl]butyl}benzyl)-4-pyrrolidinopyridinium bromide

: 73-24-5,71660-29-2,71660-30-5
7H-purin-6-ylamine

: 1365671-67-5
1-[4-(4-{4-[(6-amino-9H-purin-9-yl)methyl]phenyl}butyl)benzyl]-4-pyrrolidinopyridinium bromide

: 1365671-82-4
1-[4-(4-{4-[(6-amino-3H-purin-3-yl)methyl]phenyl}butyl)benzyl]-4-pyrrolidinopyridinium bromide

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 130 ℃; for 0.5h; Microwave irradiation;
DOI:10.1016/j.ejmech.2012.01.050

Reference yield:

: 1083-56-3
1,4-diphenylbutane

: 1365671-67-5
1-[4-(4-{4-[(6-amino-9H-purin-9-yl)methyl]phenyl}butyl)benzyl]-4-pyrrolidinopyridinium bromide

: 1365671-82-4
1-[4-(4-{4-[(6-amino-3H-purin-3-yl)methyl]phenyl}butyl)benzyl]-4-pyrrolidinopyridinium bromide

Guidance literature:: Multi-step reaction with 3 steps

1: phosphoric acid; hydrogen bromide

2: butanone / 3 h / 20 °C

3: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 130 °C / Microwave irradiation

With phosphoric acid; hydrogen bromide; potassium carbonate; In N,N-dimethyl-formamide; butanone;
DOI:10.1016/j.ejmech.2012.01.050

Reference yield:

: 886-65-7,538-81-8
trans,trans-1,4-Diphenyl-1,3-butadiene

: 1365671-67-5
1-[4-(4-{4-[(6-amino-9H-purin-9-yl)methyl]phenyl}butyl)benzyl]-4-pyrrolidinopyridinium bromide

: 1365671-82-4
1-[4-(4-{4-[(6-amino-3H-purin-3-yl)methyl]phenyl}butyl)benzyl]-4-pyrrolidinopyridinium bromide

Guidance literature:: Multi-step reaction with 4 steps

1: palladium on activated charcoal; acetic acid

2: phosphoric acid; hydrogen bromide

3: butanone / 3 h / 20 °C

4: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 130 °C / Microwave irradiation

With phosphoric acid; palladium on activated charcoal; hydrogen bromide; potassium carbonate; acetic acid; In N,N-dimethyl-formamide; butanone;
DOI:10.1016/j.ejmech.2012.01.050