methyl (S)-2-(2-((tert-butoxycarbonyl)amino)-3-phenylpropanamido)benzoate

Base Information

• Chemical Name: methyl (S)-2-(2-((tert-butoxycarbonyl)amino)-3-phenylpropanamido)benzoate
• CAS No.: 119422-44-5
• Molecular Formula: C₂₂H₂₆N₂O₅
• Molecular Weight: 398.459

Synonyms:methyl (S)-2-(2-((tert-butoxycarbonyl)amino)-3-phenylpropanamido)benzoate

Chemical Property of methyl (S)-2-(2-((tert-butoxycarbonyl)amino)-3-phenylpropanamido)benzoate

Chemical Property:

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Technology Process of methyl (S)-2-(2-((tert-butoxycarbonyl)amino)-3-phenylpropanamido)benzoate

There total 1 articles about methyl (S)-2-(2-((tert-butoxycarbonyl)amino)-3-phenylpropanamido)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

N-tert-butoxycarbonyl-L-phenylalanine (13734-34-4) + 2-carbomethoxyaniline (134-20-3) → methyl (S)-2-(2-((tert-butoxycarbonyl)amino)-3-phenylpropanamido)benzoate (119422-44-5)

Guidance literature:

N-tert-butoxycarbonyl-L-phenylalanine; With 4-methyl-morpholine; 1-hydroxy-7-aza-benzotriazole; In dichloromethane; at 0 ℃; for 0.166667h; Inert atmosphere;

2-carbomethoxyaniline; With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 7h; Inert atmosphere;

DOI:10.1039/c6ob00693k

Reference yield: 91.45%

methyl (S)-2-(2-((tert-butoxycarbonyl)amino)-3-phenylpropanamido)benzoate (119422-44-5) → Boc-Phe-Anthra-OH (123470-80-4)

Guidance literature:

With methanol; sodium hydroxide; for 10h;

DOI:10.1021/cg201268x

Reference yield:

methyl (S)-2-(2-((tert-butoxycarbonyl)amino)-3-phenylpropanamido)benzoate (119422-44-5) → C17H18N2O3

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; for 0.666667h; Inert atmosphere;

DOI:10.1039/c6ob00693k

upstream raw materials:

N-tert-butoxycarbonyl-L-phenylalanine

2-carbomethoxyaniline

Downstream raw materials:

Boc-Phe-Anthra-OH

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