1-bromo-3-methoxy-4-propoxy-5-iodobenzene

Base Information

Chemical Name:1-bromo-3-methoxy-4-propoxy-5-iodobenzene
CAS No.:481725-12-6
Molecular Formula:C₁₀H₁₂BrIO₂
Molecular Weight:371.013
Hs Code.:

Synonyms:1-bromo-3-methoxy-4-propoxy-5-iodobenzene

Suppliers and Price of 1-bromo-3-methoxy-4-propoxy-5-iodobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-bromo-3-methoxy-4-propoxy-5-iodobenzene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-bromo-3-methoxy-4-propoxy-5-iodobenzene

There total 4 articles about 1-bromo-3-methoxy-4-propoxy-5-iodobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5438-36-8
5-iodovaniline

: 481725-12-6
1-bromo-3-methoxy-4-propoxy-5-iodobenzene

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / cesium carbonate / dimethylformamide / 2 h / 50 °C

2: 91 percent / 2-methyl-2-butene; aq. sodium chlorite; NaH₂PO₄ / 2-methyl-propan-2-ol / 4 h / 20 °C

3: oxalyl chloride / dimethylformamide; CH₂Cl₂ / 18 h / 20 °C

4: 1.6 g / 2-mercaptopyridine oxide sodium salt; BrCCl₃; AIBN / 0.08 h / Heating

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; oxalyl dichloride; 2,2'-azobis(isobutyronitrile); Bromotrichloromethane; 2-mercaptopyridine-1-oxide sodium salt; caesium carbonate; In dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1016/S0957-4166(02)00334-8

Reference yield:

: 106331-89-9
3-methoxy-4-n-propyloxy-5-iodobenzaldehyde

: 481725-12-6
1-bromo-3-methoxy-4-propoxy-5-iodobenzene

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / 2-methyl-2-butene; aq. sodium chlorite; NaH₂PO₄ / 2-methyl-propan-2-ol / 4 h / 20 °C

2: oxalyl chloride / dimethylformamide; CH₂Cl₂ / 18 h / 20 °C

3: 1.6 g / 2-mercaptopyridine oxide sodium salt; BrCCl₃; AIBN / 0.08 h / Heating

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; oxalyl dichloride; 2,2'-azobis(isobutyronitrile); Bromotrichloromethane; 2-mercaptopyridine-1-oxide sodium salt; In dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1016/S0957-4166(02)00334-8

Reference yield:

: 145399-74-2
3-methoxy-4-propoxy-5-iodobenzoic acid

: 481725-12-6
1-bromo-3-methoxy-4-propoxy-5-iodobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl chloride / dimethylformamide; CH₂Cl₂ / 18 h / 20 °C

2: 1.6 g / 2-mercaptopyridine oxide sodium salt; BrCCl₃; AIBN / 0.08 h / Heating

With oxalyl dichloride; 2,2'-azobis(isobutyronitrile); Bromotrichloromethane; 2-mercaptopyridine-1-oxide sodium salt; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0957-4166(02)00334-8