methyl 2-(((tert-butyldimethylsilyl)oxy)(4-chlorophenyl)methyl)acrylate

Base Information

Chemical Name:methyl 2-(((tert-butyldimethylsilyl)oxy)(4-chlorophenyl)methyl)acrylate
CAS No.:281195-10-6
Molecular Formula:C₁₇H₂₅ClO₃Si
Molecular Weight:340.922
Hs Code.:

Synonyms:methyl 2-(((tert-butyldimethylsilyl)oxy)(4-chlorophenyl)methyl)acrylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2-(((tert-butyldimethylsilyl)oxy)(4-chlorophenyl)methyl)acrylate

Chemical Property:

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Technology Process of methyl 2-(((tert-butyldimethylsilyl)oxy)(4-chlorophenyl)methyl)acrylate

There total 3 articles about methyl 2-(((tert-butyldimethylsilyl)oxy)(4-chlorophenyl)methyl)acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 69739-34-0
t-butyldimethylsiyl triflate

: 131469-67-5
methyl 2-[1-hydroxy-1-(4-chlorophenyl)methyl]acrylate

: 281195-10-6
methyl 2-(((tert-butyldimethylsilyl)oxy)(4-chlorophenyl)methyl)acrylate

Guidance literature:: With triethylamine;
DOI:10.1016/j.tet.2012.10.057

Reference yield: 90.0%

: 131469-67-5
methyl 2-[1-hydroxy-1-(4-chlorophenyl)methyl]acrylate

: 18162-48-6
tert-butyldimethylsilyl chloride

: 281195-10-6
methyl 2-(((tert-butyldimethylsilyl)oxy)(4-chlorophenyl)methyl)acrylate

Guidance literature:: With lithium sulfide; In acetonitrile; for 5h;
DOI:10.1080/10426500490485291

Reference yield:

: 104-88-1
4-chlorobenzaldehyde

: 281195-10-6
methyl 2-(((tert-butyldimethylsilyl)oxy)(4-chlorophenyl)methyl)acrylate

Guidance literature:: Multi-step reaction with 2 steps

1: 1,4-diaza-bicyclo[2.2.2]octane

2: triethylamine

With 1,4-diaza-bicyclo[2.2.2]octane; triethylamine; 1: |Morita-Baylis-Hillman Alkylation;
DOI:10.1016/j.tet.2012.10.057